Synthesis of ZnS nanorods by a surfactant-assisted soft chemistry method
Synthesis of ZnS nanorods by a surfactant-assisted soft chemistry method
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DOI：
10.1016/s1387-7003(03)00146-1
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发表时间：
2003-07-01
影响因子：
3.8
通讯作者：
Huang, RI
中科院分区：
文献类型：
--
作者：
Zhao, QT;Hou, LS;Huang, RI
以乙二胺为双齿配体，采用溶剂热法合成了锌纳米棒，并与十二烷基硫醇形成了锌配合物，有效地控制了硫化锌纳米棒的晶体生长。得到的硫化锌纳米棒的直径和长度分别约为40 nm和1.0-1.5微米。用X射线衍射仪、透射电子显微镜和能谱仪对纳米棒的微观结构和组成进行了表征。并用光致发光光谱(PL)检测了纳米棒的光学性质。(C)2003 Elsevier Science B.V.保留所有权利。
ZnS nanorods were synthesized using solvothermal process with ethylenediamine as a bidentate ligand to form Zn2+ complexes and dodecylthiol providing an effective control over the crystal growth of ZnS nanorod. The diameter and length of ZnS nanorods obtained are similar to40 nm and 1.0-1.5 mum, respectively. The microstructure and composition of the nanorods were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and energy dispersive spectroscopy (EDS). And the optical properties of ZnS nanorods were examined by photoluminescence (PL) spectrum. (C) 2003 Elsevier Science B.V. All rights reserved.