A high-sensitivity differential scanning calorimeter with magnetic field for magnetostructural transitions

A high-sensitivity differential scanning calorimeter with magnetic field for magnetostructural transitions
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DOI:
10.1063/1.1614857
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发表时间:
2003-10
影响因子:
1.6
通讯作者:
J. Marcos;F. Casanova;X. Batlle;A. Labarta;A. Planes;L. Mañosa
J. Marcos;F. Casanova;X. Batlle;A. Labarta;A. Planes;L. Mañosa
中科院分区:
工程技术4区
文献类型:
--
作者:
J. Marcos;F. Casanova;X. Batlle;A. Labarta;A. Planes;L. Mañosa

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我们开发了一种能够在高达 5 T 的外加磁场下工作的差示扫描量热计。该量热计灵敏度很高,工作温度范围为 10-300 K。结果表明,经过适当的校准后,该系统能够测定一级固-固相变中的潜热和熵变。该系统对于研究因磁结构相变而表现出巨磁热效应的材料特别有用。给出了 Gd5(Si0.1Ge0.9)4 的数据。
We have developed a differential scanning calorimeter capable of working under applied magnetic fields of up to 5 T. The calorimeter is highly sensitive and operates over the temperature range 10–300 K. It is shown that, after a proper calibration, the system enables determination of the latent heat and entropy changes in first-order solid–solid phase transitions. The system is particularly useful for investigating materials that exhibit the giant magnetocaloric effect arising from a magnetostructural phase transition. Data for Gd5(Si0.1Ge0.9)4 are presented.