Growth of Single Crystal Film of One-Dimensional 9, 10-Dichloroanthracene

Growth of Single Crystal Film of One-Dimensional 9, 10-Dichloroanthracene
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一维9, 10-二氯蒽单晶薄膜的生长

DOI:
10.1143/jjap.19.1837
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发表时间:
1980
影响因子:
1.5
通讯作者:
K. Tomioka
K. Tomioka
中科院分区:
物理与天体物理4区
文献类型:
--
作者:
A. Matsui;K. Tomioka

文献摘要

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9,10 -二氯蒽的单晶膜生长在放置在容器底部的玻璃或熔融石英板上,容器最初填充了80%体积的饱和9,10 -二氯蒽的苯溶液。通过室温下苯的缓慢蒸发,9,10 -二氯蒽从板的上端沉积在板的两个表面上。最大的表面积约为5×7 mm2。薄膜表面的法线方向与晶体学b轴平行。反射光谱和吸收光谱的总体特征(峰位置和相对峰高)与已发表的小单晶测量数据一致。
Single crystal film of 9, 10-dichloroanthracene is grown on a glass or fused quartz plate placed at the bottom of a vessel filled initially to 80% of its volume with benzene solution saturated with 9, 10-dichloroanthracene. By slow evaporation of the benzene at room temperature, 9, 10-dichloroanthracene deposits on both surfaces of the plate from its upper end. The largest surface area is about 5×7 mm2. The normal to the film surface is oriented parallel to the crystallographic b-axis. The gross features of the reflectance and absorption spectra (the peak position and the relative peak height) are consistent with published data measured on small single crystals.