The synthesis of micrometer- and submicrometer-size spheres of ordered mesoporous oxide MCM-41

The synthesis of micrometer- and submicrometer-size spheres of ordered mesoporous oxide MCM-41
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DOI:
10.1002/adma.19970090317
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发表时间:
1997-02-01
期刊:
影响因子:
29.4
通讯作者:
Unger, KK
Unger, KK
中科院分区:
材料科学1区
文献类型:
--
作者:
Grun, M;Lauer, I;Unger, KK

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首次合成了球形介孔材料MCM-41。通过X-射线衍射,扫描电子显微镜,和氮吸附在77 K(它提供了有关的孔隙系统的信息)的样品的表征的结果进行了说明。结果表明,球形MCM-41粒子的所有性质基本上是相同的MCM-41材料的那些由公认的方法合成。最后,未来研究的可能性进行了概述。
Spherical particles of the mesoporous material MCM-41 have been synthesized and are reported for the first time. The results of characterization of the samples by X-ray diffraction, scanning electron microscopy, and nitrogen sorption at 77 K (which provides information about the pore system) is described. It is shown that all the properties of the spherical MCM-41 particles are essentially the same as those of the MCM-41 materials synthesized by well-established methods. Finally, possibilities for future research are outlined.