The infrared spectrum and thermal analysis of zinc hydroxide nitrate

The infrared spectrum and thermal analysis of zinc hydroxide nitrate
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DOI:
10.1016/0022-4596(71)90037-5
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发表时间:
1971-05
影响因子:
3.3
通讯作者:
W. Stählin;H. Oswald
W. Stählin;H. Oswald
中科院分区:
化学3区
文献类型:
--
作者:
W. Stählin;H. Oswald

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氢氧化硝酸锌Zn 5 (OH) 8 (NO 3) 2·2H 2 O 的红外光谱在4000 至200 cm− 1 之间测量。将红外光谱获得的数据与晶体结构测定的结果进行比较。建立了热性质,并用以下尺寸的单斜晶胞索引了脱水产物 Zn 5 (OH) 8 (NO 3) 2 的 X 射线粉末图:a= 17.92 (1) A ̊、b= 6.283 (3) A ̊、c= 5.391 (2) A ̊ 和 β= 91.14 (5)°。
The infrared spectrum of zinc hydroxide nitrate, Zn 5 (OH) 8 (NO 3) 2· 2H 2 O, is measured between 4000 and 200 cm− 1. The data obtained by ir spectroscopy are compared with the results of the crystal structure determination. The thermal properties are established and the X-ray powder diagram of the dehydration product Zn 5 (OH) 8 (NO 3) 2 is indexed with a monoclinic unit cell of the following dimensions: a= 17.92 (1) A ̊, b= 6.283 (3) A ̊, c= 5.391 (2) A ̊, and β= 91.14 (5)°.