Trial production of the curved crystal spectrometer for soft X-Ray Raman scattering spectroscopy
Trial production of the curved crystal spectrometer for soft X-Ray Raman scattering spectroscopy
批准号:
05554006
负责人:
NAKAI Shunichi
金额:
$10.24万
依托单位国家:
日本
项目类别:
Grant-in-Aid for Developmental Scientific Research (B)
财政年份:
1993
资助国家:
日本
项目状态:
已结题
起止时间:
1993 至 1994
中文摘要
1.软X射线拉曼散射曲晶谱仪的性能评价:(1)扫描机构的精度、可靠性和分辨率的性能测试。用电子束作为激发源。用RAP(2d=26.12A)和ADP(2d=10.64A)晶体作为分析晶体。(2)研制了光谱仪的程序控制、数据测量和处理系统。系统由PC-9800个人计算机控制。在Si-K吸收边附近测量了Si、SiO_2的共振X射线发射谱(RXES)和Si-KLL共振俄歇谱(RAS),在Y-LM吸收边测量了Y-1MMRAS对金属Y、YF_3和YCl3的影响。观察到在吸收峰能量处光谱强度共振增加,峰值能量随入射光子能量的变化呈现线性色散。此外,这些线条的形状是不对称的。因此,这些现象是由X射线共振拉曼散射引起的。
英文摘要
1.Performance evaluation of the curved crystal spectrometer for soft X-Ray Raman scattering spectroscopy.(1) Performance test for precision and reliability of a scanning mechanism and resolution of the spectrometer. An electron beam was used as an excitation source. RAP(2d=26.12A)and ADP(2d=10.64A)crystals were used as an analyzing crystal.(2) Preparation of a program control for the speetrometer, data measuring and processing systems.Systems were controled by a personal computer (PC-9800).Measurement of the soft X-Ray Raman scattering spectra.We have measured Si-K_<alpha> Resonant X-Ray Emission Spectra (RXES) and Si-KLL Resonant Auger Spectra (RAS) in the vicinity of Si-K absorption edge for Si, SiO_2 and also Y-LMM RAS in Y-Lm absorption edge for Y metal, YF_3 and YCI_3. RXES were measureed at undulator beam line BL-2A of photon Factory. It is observed that the intensity of the spectra increases resonantly at the absorption peak energy and the peak energy exhibits linear dispersion as a function of incident photon energy. Moreover, these line shapes are asymmetry. Therefore these phenomena are owing to X-Ray resonant Raman scattering.
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S.Nakai: "Linear Dichroism in Ce 3d X-Ray Absorption of CeRh_3B_2" Physica 13. 186. 74-76 (1993)
S.Nakai:“CeRh_3B_2 的 Ce 3d X 射线吸收中的线性二色性”Physica 13. 186. 74-76 (1993)
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K.ODAGAWA: "SOFT X-RAY RESONANT RAMAN SCATTERING AND RESONANT AUGER ELECTRON SPECTROSCOPY" PHOTON FACTORY ACTIVITY REPORT. 11. 20 (1994)
K.ODAGAWA:“软 X 射线共振拉曼散射和共振螺旋电子光谱”光子工厂活动报告。
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S. Nakai: "Polarized Cu L Absorption of Bi_2Sr_2Ca_<1-x>Y_XCu_2O_8 (X=0.0,0.6)" Jpn. J. Appl. Phys. 32-2. 602-604 (1993)
S. Nakai:“Bi_2Sr_2Ca_<1-x>Y_XCu_2O_8 (X=0.0,0.6) 的极化 Cu L 吸收”Jpn。
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S.Nakai他: "Polarized Cu L Absorption of Bi_2Sr_2Ca_<1-x>Y_xCu_2O_8(x=0.0,0.6)" Jpn.J.Appl.Phys. 32-2. 602-604 (1993)
S. Nakai等:“Bi_2Sr_2Ca_<1-x>Y_xCu_2O_8(x=0.0,0.6)的极化Cu L吸收”Jpn.J.Appl.Phys 32-2(1993)。
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S.Nakai他: "Linear Dichroism in Ce 3d X-Ray Absorption of CeRh_3B_2" Physica13. 186. 74-76 (1993)
S. Nakai 等人:“CeRh_3B_2 的 Ce 3d X 射线吸收中的线性二色性”Physica13. 74-76 (1993)
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