Molten Salt Synthesis of Acicular Ba2NaNb5O15 Seed Crystals

Molten Salt Synthesis of Acicular Ba2NaNb5O15 Seed Crystals
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熔盐合成针状 Ba2NaNb5O15 晶种

DOI:
10.1111/j.1551-2916.2005.00058.x
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发表时间:
2005-02
期刊:
J. Am. Ceram. Soc.
影响因子:
--
通讯作者:
Peiling Wang
Peiling Wang
中科院分区:
其他
文献类型:
--
作者:
Qingwei Huang;Jiong Xu;Lihui Zhu;Hui Gu;Peiling Wang

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采用BaCO3、Nb2O5与NaCl熔盐反应,成功地制备了针状Ba2NaNb5O15(BNN)晶种。考察了煅烧温度、时间、氧化物与盐的质量比等因素对BNN颗粒形貌的影响。当盐与氧化物的比例为2:1时,在1200°C下反应4 h,可得到高长径比、均匀的针状晶种。
Well-developed acicular Ba2NaNb5O15 (BNN) seed crystals have been successfully prepared by the reaction between BaCO3, Nb2O5 and molten NaCl salt. The effects of the calcination temperature, time, and weight ratio of the oxide mixture to salt on the morphology of BNN particles were investigated. Uniform acicular seeds with high aspect ratio could be achieved at 1200°C for 4 h with the salt-to-oxide mixture of 2:1.
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