Synthesis and Characterization of a Tetramethyl Furanone Functionalized Diiminedioxime, A Potential Ligand for Cu Radiopharmaceuticals, and its Copper(II) and Nickel(II) Complexes.
Synthesis and Characterization of a Tetramethyl Furanone Functionalized Diiminedioxime, A Potential Ligand for Cu Radiopharmaceuticals, and its Copper(II) and Nickel(II) Complexes.
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四甲基呋喃酮功能化二亚胺二肟（Cu 放射性药物的潜在配体）及其铜 (II) 和镍 (II) 配合物的合成和表征。
DOI：
10.1016/j.poly.2008.12.006
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发表时间：
2009
期刊：
影响因子：
2.6
通讯作者：
Packard,AlanB
中科院分区：
文献类型：
--
作者：
Kiani,Salma;Staples,RichardJ;Treves,STed;Packard,AlanB
As part of our on-going effort to develop64Cu-based radiopharmaceuticals for PET (positron emission tomography) imaging of multidrug resistance in cancer, we prepared a tetramethylfuranone-functionalized diiminedioxime ligand, TMFPreH (TMFPreH=4-[3-(4-hydroxyimino-2,2,5,5-dimethyl-dihydro-furan-3-ylideneamino)-propylimino]-2,2,5,5-tetramethyl-dihydrofuran-3(2H)-one oxime) and its Cu(II) and Ni(II) complexes. When the copper(II) complex was prepared from Cu(ClO4)2in ethanol, it was isolated as a Cu(II)-bridged dimer, but when it was prepared from Cu(OAc)2and heated in acetone, an unusual example of an acetone adduct of the ligand is formed by reduction of one of the imine double bonds by the solvent. The Ni(II) complex is square pyramidal with the perchlorate counterion at the apex.
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影响因子：
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作者：
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DOI：
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发表时间：
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期刊：
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影响因子：
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发表时间：
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