Controllable synthesis of Bi2S3 hierarchical nanostructures: Effect of addition method on structures
Controllable synthesis of Bi2S3 hierarchical nanostructures: Effect of addition method on structures
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Bi2S3分级纳米结构的可控合成：添加方法对结构的影响
DOI：
10.1016/j.jallcom.2009.03.028
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发表时间：
2009-07
影响因子：
6.2
通讯作者：
Han, Qiaofeng
中科院分区：
文献类型：
--
作者：
Lu, Lude;Sun, Yan;Wang, Xin;Yang, Xujie;Chen, Liang;Han, Qiaofeng
Bi2S3microcrystallites with three-dimensional (3D) superstructures were synthesized by the reaction of bismuth nitrate (Bi(NO3)3) with sodium O-isopropyldithiocarbonate (isopropyl xanthate, C3H7OCS2Na) at 80°C in N,N-dimethylformamide (DMF) solution without any surfactants. It was observed that Bi2S3crystalline nanorods aggregated to urchin-like globules in the microscale when C3H7OCS2Na was slowly added to Bi(NO3)3in DMF solution at 80°C, while cockscomb-like microspheres aggregated by Bi2S3nanobelts with a typical width of ∼20nm were obtained if two precursors were mixed at room temperature and then heated to 80°C. Possible mechanisms for the formation of 3D Bi2S3microcrystals were proposed. The structures of Bi2S3crystals were examined by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and laser Raman spectroscopy.
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影响因子：
3.8
作者：
A. Vreugdenhil;S. Brienne;R. Markwell;I. Butler;J. Finch
通讯作者：
A. Vreugdenhil;S. Brienne;R. Markwell;I. Butler;J. Finch
影响因子：
3
作者：
Cong-Ming Tang;Guonian Wang;Huiwu Wang;Yunxia Zhang;Guanghai Li
通讯作者：
Cong-Ming Tang;Guonian Wang;Huiwu Wang;Yunxia Zhang;Guanghai Li
影响因子：
6.2
作者：
Xiaohu Huang;You-wen Yang;Xincun Dou;Yonggang Zhu;Guanghai Li
通讯作者：
Xiaohu Huang;You-wen Yang;Xincun Dou;Yonggang Zhu;Guanghai Li
影响因子：
4.6
作者：
赵仪
通讯作者：
赵仪
Bi2S3 多面纳米管束的合成与表征
影响因子：
2.1
作者：
Shen, Xiao-Ping;Yin, Gui;Xu, Zheng
通讯作者：
Xu, Zheng