Grain growth behaviour and mechanical properties of coarse-grained cemented carbides with bimodal grain size distributions

Grain growth behaviour and mechanical properties of coarse-grained cemented carbides with bimodal grain size distributions
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双峰晶粒尺寸分布粗晶硬质合金的晶粒长大行为和力学性能

DOI:
10.1016/j.msea.2020.140586
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发表时间:
2020-11
影响因子:
6.4
通讯作者:
Ruan Jianming
Ruan Jianming
中科院分区:
材料科学1区
文献类型:
--
作者:
He Rengui;Yang Qiumin;Li Bin;Lou Jia;Yang Hailin;Ruan Jianming

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采用精确控制WC粒度分布的WC-5Co复合粉末,研究了具有双晶粒度分布的粗晶硬质合金的WC晶粒长大行为和力学性能。采用Sol-Gel法制备了复合粉末,并在粗WC(C-WC,6.0gμm)中加入超细WC(UF-WC,300 nm)以调节WC的粒度分布。结果表明,当UF-WC加入量较低(≤6%)时,WC颗粒呈二维形核长大,呈截断的三棱柱状;而当UF-WC加入量较高(≥9%)时,WC颗粒以三维形核长大,呈金字塔状,具有层层结构。维氏硬度和断裂韧性测试表明,含6wt%UF-WC的硬质合金硬度(1281.7±11.6)HV_(10)和断裂韧性(25.4±0.2)Mpa·M~(1/2)均有显著提高。
The WC grain growth behaviour and mechanical properties of coarse-grained cemented carbides with bimodal grain size distributions were investigated using WC-5Co composite powders with accurately controlled WC grain size distribution. The composite powders were prepared by a Sol-Gel process and ultrafine WC (UF-WC, 300 nm) was added to coarse WC (C-WC, 6.0 μm) to adjust the WC grain size distribution. It indicated that the WC grains undergo 2-D nucleation with 2-D growth at low UF-WC addition (≤6 wt%), resulting in a truncated trigonal prisms shape, whereas the WC grains grow up through 2-D nucleation with 3-D growth at high UF-WC addition (≥9 wt%), leading to a pyramid-like shape with a layer-by-layer structure of WC grains. Vickers hardness and fracture toughness tests indicated that the cemented carbide containing 6 wt% UF-WC present significant improvements in the hardness (1281.7 ± 1.6 HV10) and the fracture toughness (25.4 ± 0.2 MPa m1/2).
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