Solvothermal growth of NiS single-crystalline nanorods
Solvothermal growth of NiS single-crystalline nanorods
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NiS单晶纳米棒的溶剂热生长
DOI:
10.1016/j.jallcom.2009.02.154
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发表时间:
2009-07
影响因子:
6.2
通讯作者:
Wu, R.
中科院分区:
文献类型:
--
作者:
Yang, Pengfei;Zheng, Yufeng;Jian, J. K.;Sun, Yanfei;Song, B.;Wu, R.
Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200°C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80nm to 120nm, and from 2μm to 3μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.
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