Solvothermal growth of NiS single-crystalline nanorods

Solvothermal growth of NiS single-crystalline nanorods
复制标题

NiS单晶纳米棒的溶剂热生长

DOI:
10.1016/j.jallcom.2009.02.154
复制
发表时间:
2009-07
影响因子:
6.2
通讯作者:
Wu, R.
Wu, R.
中科院分区:
材料科学2区
文献类型:
--
作者:
Yang, Pengfei;Zheng, Yufeng;Jian, J. K.;Sun, Yanfei;Song, B.;Wu, R.

文献摘要

参考文献

相似文献

以硫和镍粉为原料,乙二胺为溶剂,在200°C下采用溶剂热法成功制备了NiS纳米棒。采用X射线衍射(XRD)、场发射扫描电子显微镜(FE-SEM)和透射电子显微镜(TEM)对NiS纳米棒进行了表征。结果表明,纳米棒的直径在80 ~ 120 nm之间,长度在2 ~ 3μm之间。NiS纳米棒是具有尖晶石结构的单晶。在实验结果和相关文献的基础上,讨论了NiS纳米棒晶体的可能生长机制。
Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200°C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80nm to 120nm, and from 2μm to 3μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.
DOI: 10.1016/s0925-8388(03)00380-3
发表时间: 2003-10-27
影响因子: 6.2
作者:
Han, SC;Kim, KW;Lee, JY
通讯作者: Lee, JY
DOI: 10.1006/jssc.2002.9556
发表时间: 2002-06
影响因子: 5.4
作者:
Zhengping Qiao;Gang Xie;J. Tao;Zhao-Yang Nie;Yan-Zhi Lin;Xiao‐Ming Chen
通讯作者: Zhengping Qiao;Gang Xie;J. Tao;Zhao-Yang Nie;Yan-Zhi Lin;Xiao‐Ming Chen
DOI: 10.1021/cm970789l
发表时间: 1998-09-01
影响因子: 8.6
作者:
Li, YD;Liao, HW;Zhou, GE
通讯作者: Zhou, GE
DOI: 10.1016/s1387-7003(03)00146-1
发表时间: 2003-07-01
影响因子: 3.8
作者:
Zhao, QT;Hou, LS;Huang, RI
通讯作者: Huang, RI
DOI: 10.1021/ja0484505
发表时间: 2004-07-07
影响因子: 15
作者:
Zhang, LZ;Yu, JC;Kwong, KW
通讯作者: Kwong, KW