Synthesis and Characterization of Water-Soluble Monolayer-Protected Gold Nanoparticles

Synthesis and Characterization of Water-Soluble Monolayer-Protected Gold Nanoparticles
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水溶性单层保护金纳米粒子的合成与表征

DOI:
10.4028/www.scientific.net/amr.415-417.617
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发表时间:
2011
期刊:
Advanced Materials Research
影响因子:
--
通讯作者:
Martin M. F. Choi
Martin M. F. Choi
中科院分区:
--
文献类型:
--
作者:
Yan Su;Y. Lin;Yuyao Fu;Fan Qian;Xiupei Yang;Martin M. F. Choi

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以2-巯基-4-甲基-5-噻唑乙酸(MMTA)为稳定剂,硼氢化钠(NaBH 4)为还原剂制备了水溶性金纳米粒子(AuNPs)。通过透射电子显微镜(TEM)、紫外-可见吸收光谱和傅里叶变换红外光谱(FTIR)对AuNPs产物进行分析。TEM图像显示颗粒分散良好,其平均粒径约为5 nm。UV-vis吸收和FTIR光谱证实MMTA-AuNP被存在于AuNP表面上的羧酸根离子稳定。
Water-soluble gold nanoparticles (AuNPs) were prepared using 2-mercapto-4-methyl-5- thiazoleacetic acid (MMTA) as a stabilizing agent and sodium borohydride (NaBH4) as a reducing agent. The AuNPs product was analyzed by transmission electron microscopy (TEM), UV-vis absorption spectroscopy and Fourier transform infrared spectroscopy (FTIR). The TEM image shows that the particles were well-dispersed and their average particle size is about 5 nm. The UV-vis absorption and FTIR spectra confirm that the MMTA-AuNPs was stabilized by the carboxylate ions present on the surface of the AuNPs.
DOI: 10.1021/ac015657x
发表时间: 2002-02-01
影响因子: 7.4
作者:
Nath, N;Chilkoti, A
通讯作者: Chilkoti, A