Acquisition of a Gradient High Performance Liquid Chromatograph and Fourier-Transform Infrared Spectrometer for Investigation of Stereoselective Nitroaldol (Henry) Reactions

购买梯度高效液相色谱仪和傅里叶变换红外光谱仪来研究立体选择性硝基羟醛（亨利）反应

• 批准号: 0321234
• 负责人: Lawrence McGahey
• 金额: $ 3.83万
• 依托单位: College of Saint Scholastica
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 2003
• 资助国家: 美国
• 起止时间: 2003-08-01 至 2006-07-31
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=0321234&HistoricalAwards=false
• 关键词: Acquisition; Gradient; Performance; Liquid; Chromatograph

With support from the Major Research Instrumentation (MRI) Program, the Department of Chemistry at the College of St. Scholastica will acquire a gradient high performance liquid chromatograph (HPLC) and Fourier-transform infrared (FTIR) spectrometer. This equipment will enable investigations of stereoselective nitroaldol (Henry) reactions. High performance liquid chromatography is an extremely powerful technique used for the separation and analysis of complex mixtures. A Fourier transform infrared spectrometer is a veritable workhorse in the modern chemical laboratory and can provide important information about molecular and electronic structure. This research should add to the field of synthetic chemistry and it will teach and train undergraduates in the area of synthetic chemistry and in the operation of HPLC and FTIR instruments.

在主要研究仪器（MRI）项目的支持下，圣斯考拉西卡学院化学系将获得一台梯度高效液相色谱仪（HPLC）和傅里叶变换红外光谱仪（FTIR）。该设备将使立体选择性硝基醇（亨利）反应的研究成为可能。高效液相色谱是一种非常强大的技术，用于分离和分析复杂的混合物。傅里叶变换红外光谱仪是现代化学实验室中名副其实的主力仪器，它能提供有关分子和电子结构的重要信息。这项研究应该是对合成化学领域的补充，它将教授和培训合成化学领域的本科生以及HPLC和FTIR仪器的操作。