Investigation of Ultra Faster Melting Process of Very Fine High-Polymer Particle.

极细高分子颗粒超快熔化过程的研究。

• 批准号: 03650179
• 负责人: KUMADA Masaya
• 金额: $ 1.34万
• 依托单位: Gifu University, Faculty of Engineering
• 依托单位国家: 日本
• 项目类别: Grant-in-Aid for General Scientific Research (C)
• 财政年份: 1991
• 资助国家: 日本
• 起止时间: 1991 至 1992
• 项目状态: 已结题
• 来源: https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-03650179/
• 关键词: Fine Particle; High-Polymer; Faster Melt-Process; Non-Newtonian; Penetrating; Heat Plastic Nature; Image Processing; トナ-; 融解; 凝固; 高分子ポリマ-; 画像処理; 透過率; 〓射加熱; レ-ザ-光

In order to improve the print speed of Laser Beam Printer with flash heating, the clarification of phenomena in the melting process of a high polymer particle by flash heating has become very important in recent years. But, almost no theoretical and phenomenological explanations are given about this melting mechanism, because there are the rheological, phase change and the heat transfer problems in this melting process; that is, the temperature of a particle becomes over the melting point, the phase change from solid to liquid partially happen. The natural convection will proceed inside the particle in step with the liquefied. Finally, deformation of the polymer particle will be occurred by fluidity of fusing polymer and power balance between gravity and surface tension onto the material on which the polymer particle is put.From this viewpoint, the present study as the first stage was designed to clarify the external deformation process of a high polymer particle under the condition of … More continuous radiant heating. Furthermore, in order to clarify a melting process inside the polymer particle, the method of measuring the moving of the interface between solid and liquid was investigated.The heating source is used a xenon lamp ( max. 150W ) which can be controlled the power and the exposure time. The beam is converged by a reflector to in 5mm diameter with flat distribution. The polymer particle used in the present study is one kind of acrylic polymer and its shape is spherical. The diameter of particles are 0.15-0.5mm which are 30-100 times. as large as real toner particles. The melting process is observed by a micro-scope and a CCD camera, and the continuous pictures are stored by video. The recorded pictures are digitalized to pixels ( 512x512 ) and light degrees ( 256 ) by the image board and transfer on memory of microcomputer for analysis.The focused laser beam is used in the measurement for moving of inter-face and the light intensity of laser beam penetrated the particle is measured by a semi-conductor transducer, and digitized by A-D transducer board to transfer to micro-computer for analysis.The results show that the external deformation pattern of a polymer particle with time is apparently similar regardless of the size of particle and radiant heating power. But, the deformation process is not monotonous with time and shows the singular point corresponding to progress of melting (that is, interface between solid and liquid). The method of measuring for moving of the interface by using laser beam was proved effective. The results are agreed with one of simulation qualitatively. Less

为了提高激光束打印机的闪光加热打印速度，近年来澄清高聚物颗粒通过闪光加热熔化过程中的现象变得非常重要。但是，由于熔化过程中存在流变、相变和传热问题，因此几乎没有对这种熔化机制给出理论和现象学的解释；也就是说，颗粒的温度超过熔点，部分发生从固态到液态的相变。自然对流将在颗粒内部与液化同步进行。最后，聚合物颗粒的变形将通过熔融聚合物的流动性以及聚合物颗粒所放置的材料上的重力和表面张力之间的力平衡而发生。从这个角度来看，本研究作为第一阶段旨在阐明高聚物颗粒在连续辐射加热条件下的外部变形过程。此外，为了阐明聚合物颗粒内部的熔融过程，研究了测量固液界面移动的方法。加热源采用氙灯（最大150W），可以控制功率和曝光时间。光束经反射镜会聚至直径为 5mm 的平面分布。本研究中使用的聚合物颗粒是一种丙烯酸聚合物，其形状为球形。颗粒直径为0.15-0.5mm，为30-100倍。与真正的墨粉颗粒一样大。通过显微镜和CCD相机观察熔化过程，并通过视频存储连续图片。记录的图像通过图像板数字化为像素（512x512）和光度（256）并传输到微机内存中进行分析。采用聚焦激光束测量界面移动，通过半导体传感器测量激光束穿透颗粒的光强，并通过A-D传感器板数字化传输到微机进行分析。 结果表明，无论颗粒尺寸和辐射加热功率如何，聚合物颗粒随时间的外部变形模式明显相似。但是，变形过程随着时间的推移并不单调，并显示出与熔化过程相对应的奇点（即固体和液体之间的界面）。利用激光束测量界面移动的方法被证明是有效的。结果在定性上与模拟结果一致。较少的

项目成果

Jyuniji Mimatsu: "Melting Process of a Fine Polymer Particle by Flash Heating" Procs.of Int.Seminar on Imaging in Transport Processes Athens,Greece,May 25ー29,1992.

Jyuniji Mimatsu：“通过快速加热熔化细聚合物颗粒”Procs.of Int.Seminar on Imaging in Transport Processes 雅典，希腊，1992 年 5 月 25-29 日。

Junji MIMATSU and Masaya KUMADA: "Investigation of High-Speed Melting process of Fine High-Polymer Particle." Procs. of 29th Japan Heat Transfer Symposium. 779-780 (1992)

Junji MIMATSU 和 Masaya KUMADA：“精细高分子颗粒高速熔化过程的研究”。

Junji Mimatu Masaya Kumada: "Melting Process of Fine Polyme Particle by Flash Heating(External Deformation of a Polymer Particle Heated by Steady Radiant Light)" Procs.of INTERNATIONAL CENTER FOR HEAT and MASS TRANSFER(IMAGING IN TRANSPORT PROCESSES). 13-

Junji Mimatu Masaya Kumada：“通过快速加热实现细小聚合物颗粒的熔化过程（通过稳定辐射光加热的聚合物颗粒的外部变形）”Procs.of 国际热与传质中心（运输过程中的成像）。

三松 順治 熊田 雅彌: "高分子ポリマー微小粒子の融解過程の解明(粒子外形の時間変化の画像処理による定量化)" 第29回日本伝熱シンポジウム講演論文集. 779-780 (1992)

Junji Mimatsu 和 Masaya Kumada：“阐明聚合物微粒的熔化过程（通过图像处理量化颗粒外部形状的时间变化）”第 29 届日本传热研讨会论文集 779-780（1992 年）。

Junji Mimatu,Masya Kumada: "Melting Process of Fine Polyme Particle by Flash Heating (External Deformation of a Polymer Particle Heated by Steady Radiant Light)" Procs.of INTERNATIONAL CENTER FOR HEAT and MASS TRANSFER (IMAGING IN TRANSPORT PROCESSES). 13

Junji Mimatu、Masya Kumada：“通过快速加热实现细小聚合物颗粒的熔化过程（通过稳定辐射光加热的聚合物颗粒的外部变形）”Procs.of 国际传热传质中心（运输过程中的成像）。