Probing the nanomechanics of single grain boundary with decorated solutes

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Grain boundaries (GBs) are thermodynamically susceptible to attract solutes to reduce system energy. Elaborately manipulating the GB nanostructure and chemistry via segregation can essentially be conducive, rather than detrimental, to materials performance. However, the underlying mechanism of GB segregation and its detailed effect on material properties remain elusive due to the GB complexities in the polycrystals. Through correlative in-situ nanomechanical testing and atom probe tomography, this project aims to unravel the rationale of segregation behaviour of individual GBs and its effectiveness to enhance the material performance, and hence enable nanostructural design of advanced metallic materials with unprecedented properties.