A double length inert-atmosphere glove box

双长惰性气氛手套箱

• 批准号: 344949-2007
• 负责人: Gates, Derek
• 金额: $ 5.32万
• 依托单位: University of British Columbia
• 依托单位国家: 加拿大
• 项目类别: Research Tools and Instruments - Category 1 (<$150,000)
• 财政年份: 2006
• 资助国家: 加拿大
• 起止时间: 2006-01-01 至 2007-12-31
• 项目状态: 已结题
• 来源: https://www.nserc-crsng.gc.ca/ase-oro/Details-Detailles_eng.asp?id=325886
• 关键词: double; length; inert; atmosphere; glove

This research tools and instruments application is for a double-length inert-atmosphere glovebox which is essential to perform the PI's NSERC-funded research in inorganic and polymer chemistry.  This equipment, which is standard in many synthetic laboratories, is used to store and manipulate  highly air/moisture-sensitive chemicals. Acquisition of the requested equipment will facilitate the synthesis and study of unusual phosphorus containing molecules, polymers and catalysts. The polymers may find application as electronic materials and polymer-supported catalysts. In addition, new P=C ligands are being developed for metal-catalyzed asymmetric organic synthesis.  The current facilities in the PI's lab are inadequate and do not provide enough space for the nine researchers working on this chemistry. A double-length glovebox with four gloves is urgently needed and will dramatically increase the laboratory's research productivity by allowing two additional researchers to work concurrently. The glovebox will be equipped with a temperature controlling unit and a freezer that will facilitating the handling of thermally sensitive and pyrophoric materials. Additionally, a cold well will allow for low-temperature reactions.

该研究工具和仪器应用于双长度惰性气氛手套箱，这对于执行PI的nserc资助的无机和聚合物化学研究至关重要。该设备是许多合成实验室的标准设备，用于存储和操作高度空气/湿度敏感的化学品。获得所需的设备将有助于合成和研究不寻常的含磷分子、聚合物和催化剂。该聚合物可作为电子材料和聚合物负载催化剂。此外，新的P=C配体也被开发用于金属催化的不对称有机合成。目前，PI实验室的设备不足，无法为从事这种化学研究的9名研究人员提供足够的空间。目前迫切需要一个有4只手套的双长度手套箱，这将极大地提高实验室的研究效率，因为它允许另外两名研究人员同时工作。手套箱将配备温度控制装置和冷冻室，以方便处理热敏性和热敏性材料。此外，冷井可以进行低温反应。