Control and optimal operation of the reductive amination and of the hydroaminomethylation in the demonstration plants (D04*)

子项目D4 N的重点是开发和应用示范工厂的优化过程控制概念，特别注意不确定性。推导了两个微型工厂（TMS和MLS）的动态模型，量化了不确定性，并对过程设计的可控性（D1N）进行了评价。作为小型工厂最佳运行的基础，设计和测试了数据重构和状态估计技术，考虑到不同测量的采样率差异很大。控制概念基于迭代稳态优化和模型预测控制的组合，以及机会约束动态实时优化。

Subproject D4 N focuses on the development and application of optimizing process control con-cepts for the demonstration plants with special attention to uncertainties. Dynamic models are de-rived for both miniplants (TMS & MLS), the uncertainties are quantified, and the controllability of pro-cess designs (D1 N) is evaluated. As a basis for the optimal operation of the mini-plants, data recon-ciliation and state estimation techniques are designed and tested, taking into account the largely dif-ferent sampling rates of different measurements. The control concepts are based on a combination of iterative steady-state optimization and model predictive control, and on chance-constrained dy-namic real-time optimization.