Continuous Cold without Cryogenic Consumables: Development of a Convenient Laboratory Tool for Low-Temperature Flow Processes

Continuous Cold without Cryogenic Consumables: Development of a Convenient Laboratory Tool for Low-Temperature Flow Processes
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无需低温耗材的连续冷却:开发用于低温流动过程的便捷实验室工具

DOI:
10.1002/ceat.201200581
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发表时间:
2013
影响因子:
2.1
通讯作者:
Browne D
Browne D
中科院分区:
工程技术4区
文献类型:
--
作者:
Browne D

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为了激励更多的合成化学家采用连续流化学处理技术,需要克服许多挑战。举例来说,使用低温消耗品来冷却反应在规模上或在延长的反应时间上是不切实际的。在此,通过开发一种方便的实验室设备来描述该问题的解决方案,该设备使用精确的热能传递块,为化学家提供连续流处理的好处,该热能传递块提供长期反应稳定性,并且不会进水。
There are a number of challenges that need to be overcome in order to stimulate more synthesis chemists to adopt continuous‐flow chemical processing techniques. By way of example, the use of cryogenic consumables to cool reactions is impractical on scale or over extended reaction times. Here, a solution to the problem is described with the development of a convenient laboratory device that offers chemists the benefits of continuous flow processing using an accurate thermal energy transfer block which provides long‐term reaction stability and is free from water ingress.
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