Synthesis of high-purity bulk Ti2AlN by spark plasma sintering (SPS)

Synthesis of high-purity bulk Ti2AlN by spark plasma sintering (SPS)
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放电等离子烧结 (SPS) 合成高纯块状 Ti2AlN

DOI:
10.1016/j.ceramint.2007.04.009
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发表时间:
2008-08
影响因子:
5.2
通讯作者:
--
中科院分区:
材料科学1区
文献类型:
--
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Single-phase bulk Ti2AlN was prepared by spark plasma sintering (SPS) at 1200°C of Ti/Al/TiN powders in stoichiometric proportion. Investigated by X-ray diffraction (XRD) of samples and the sintering process parameter, the reaction procedure could be analyzed. Scanning electron microscopy (SEM) and electron probe micro-analysis (EPMA) coupled with energy-dispersive spectroscopy (EDS) were utilized to investigate the morphology characteristics. When sintered at 1200°C, Ti2AlN phase was well developed with a close and lamellated structure. The distribution of Ti2AlN grains was homogeneous.
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