Elemental imaging method based on a dielectric barrier discharge probe coupled with inductively coupled plasma mass spectrometry
Elemental imaging method based on a dielectric barrier discharge probe coupled with inductively coupled plasma mass spectrometry
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基于介质阻挡放电探针耦合电感耦合等离子体质谱的元素成像方法
DOI：
10.1016/j.sab.2018.05.028
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发表时间：
2018-09
期刊：
影响因子：
--
通讯作者：
Hu Shenghong
中科院分区：
文献类型：
--
作者：
Xing Zhi;Yang Meng;Guo Wei;Jin Lanlan;Liu Zhifu;Hu Shenghong
An elemental imaging method based on a dielectric barrier discharge (DBD) probe as a sputtering source coupled with inductively coupled plasma mass spectrometry (ICP-MS) has been demonstrated. The DBD probe is simple to construct and the discharge power for producing micro plasma jet at ambient condition is as low as 3.75 W. To investigate the sputtering process, the major operating parameters of this technique are demonstrated by detecting23Na,27Al,29Si,44Ca,55Mn and57Fe in rock standard reference materials GBW07108. The reproducibility of the parallel detection was 1% (n= 7) for Hg in ABS sample was obtained. Based on these conditions, the elemental imaging is successfully obtained in the lead-based glaze ceramic with206Pb,207Pb, and208Pb, Chinese seal script with202Hg and siliceous stromatolites with27Al,29Si, and44Ca. When the 100 μm capillary was used to ablate the ABS sample, the washout time of 600 ms for Hg was obtained, and the spatial resolution of 106 μm was obtained. In addition, the potential quantitative analysis of this method has been studied, which provide the detection limits of ABS samples with 252 μg g−1for52Cr, 24 μg g−1for202Hg and 167 μg g−1for208Pb, respectively. The present imaging method has the unique capabilities of multi-elemental analysis, easy set-up and low consumption, which may serve as a complementary technology for current elemental imaging technology.
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DOI：
10.1016/j.sab.2013.04.005
发表时间：
2013-07
期刊：
Spectrochimica Acta Part B: Atomic Spectroscopy
影响因子：
--
作者：
S. Müller;T. Krähling;D. Veẑa;V. Horvatić;C. Vadla;J. Franzke
通讯作者：
S. Müller;T. Krähling;D. Veẑa;V. Horvatić;C. Vadla;J. Franzke
影响因子：
7.4
作者：
Cody, RB;Laramée, JA;Durst, HD
通讯作者：
Durst, HD
DOI：
10.1016/j.scitotenv.2014.05.115
发表时间：
2014-10
期刊：
The Science of the total environment
影响因子：
--
作者：
N. McGowan;Ashley M. Fowler;K. Parkinson;D. Bishop;K. Ganio;P. Doble;D. Booth;D. Hare
通讯作者：
N. McGowan;Ashley M. Fowler;K. Parkinson;D. Bishop;K. Ganio;P. Doble;D. Booth;D. Hare
介质阻挡放电原子化器氢化物发生原子荧光光谱法同时测定砷和锑
影响因子：
3.3
作者：
Xing, Zhi;Zhang, Sichun;Han, Guojun;Wang, Juan;Kuermaiti, Biekesailike;Zhang, Xinrong
通讯作者：
Zhang, Xinrong
影响因子：
7.4
作者：
H. A. O. Wang;D. Grolimund;L. V. Van Loon;K. Barmettler;C. Borca;B. Aeschlimann;D. Günther
通讯作者：
H. A. O. Wang;D. Grolimund;L. V. Van Loon;K. Barmettler;C. Borca;B. Aeschlimann;D. Günther