Essential Oils from Citrus reticulata cv. Shatangju Peel: Optimization of Hydrodistillation Extraction by Response Surface Methodology and Evaluation of Their Specific Adhesive Effect to Polystyrene.

Essential Oils from Citrus reticulata cv. Shatangju Peel: Optimization of Hydrodistillation Extraction by Response Surface Methodology and Evaluation of Their Specific Adhesive Effect to Polystyrene.
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来自 Citrus reticulata cv. 的精油。

DOI:
10.1021/acsomega.1c00895
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发表时间:
2021-06-01
期刊:
影响因子:
4.1
通讯作者:
Dong Y
Dong Y
中科院分区:
化学3区
文献类型:
--
作者:
Cui H;Chen X;Wang L;An P;Zhou H;Dong Y

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柑橘皮精油(EO)被广泛使用,其对聚苯乙烯(PS)的粘合作用也是偶然发现的。目的:对黄连挥发油成分进行分析。采用响应面方法对沙糖菊(CrspEos)的水蒸气蒸馏提取工艺进行优化。用气相色谱-质谱法分析了CrspEos的化学组成。然后,评价了这些精油对PS的粘接效果。测定了黏附面积、黏附对材料上精油厚度的影响、黏附对PS透光率的影响、黏附点的强度、黏附的专一性。最佳提取条件为液固比为8.94:1,浸泡时间为199.45μ,提取时间为138.71 m in。挥发油的主要成分是d-柠檬烯(56.66%),其次是月桂烯(6.62%)。CrspEos对PS具有特殊的黏附作用,不影响PS的厚度和透光率,但韧性强于母材。CrspEos是一种环保型PS专用胶粘剂。
Essential oil (Eo) from the Citrus reticulata peel has been widely used, and its adhesive effect on polystyrene (PS) was found accidentally. To analyze the essential oils of C. reticulata cv. Shatangju (CrspEos), the extraction of these oils by steam distillation was optimized using the response surface method. The chemical composition of CrspEos was analyzed by gas chromatography–mass spectrometry. Then, the adhesive effect of these essential oils on PS was evaluated. The adhesion area, the influence of adhesion on the thickness of the essential oil on the materials, the effect of adhesion on the transmittance of PS, the strength of adhesion point, and specificity of adhesion were determined. The optimum extraction conditions resulting in the extraction yield of 47.37 μL g–1 were a ratio of liquid-to-solid of 8.94:1, a soaking time of 199.45 min, and an extraction time of 138.71 min. The major component in the essential oils was d-limonene (56.66%), followed by myrcene (6.62%). CrspEos presented a specific adherence effect on PS without influencing the thickness and transmittance of PS but with stronger tenacity than the parent material. CrspEos can be used as an environmentally friendly specific adhesive for PS.
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