Low-Temperature Continuous Flow Synthesis of Metal Ammonium Phosphates.

Low-Temperature Continuous Flow Synthesis of Metal Ammonium Phosphates.
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DOI:
10.1038/s41598-018-31694-x
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发表时间:
2018-09-10
期刊:
影响因子:
4.6
通讯作者:
Bond G
Bond G
中科院分区:
综合性期刊3区
文献类型:
--
作者:
Holdsworth AF;Eccles H;Halman AM;Mao R;Bond G

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对现代生活质量至关重要的高性能无机材料的合成受到传统态度和对过时方法(例如批量合成)的依赖的阻碍。虽然连续流动方法已在制药界广泛采用,但尽管其效率更高、安全性和多功能性更高,但它们在无机化合物的制备方面仍然很大程度上未经探索。在本出版物中,我们通过将现有的间歇工艺转变为低温连续工艺,展示了金属磷酸铵合成的阶跃变化,产量增加了十倍,同时粒径显着减小。
The synthesis of the high performance inorganic materials essential to the quality of modern day life is hindered by traditionalist attitudes and reliance on outdated methods such as batch syntheses. While continuous flow methods have been extensively adopted in pharmaceutical circles, they remain largely unexplored for the preparation of inorganic compounds, despite higher efficiency, safety and versatility. In this publication, we demonstrate a step-change for the synthesis of metal ammonium phosphates through conversion of the extant batch process to a low-temperature continuous regime, exhibiting a tenfold increase in throughput combined with a significant decrease in particle size.
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