Use of FT-NMR Spectroscopy in the Undergraduate Chemistry Curriculum

该项目将介绍200 MHz傅立叶 将核磁共振（FT-NMR）光谱转换为 我们的有机化学和高级实验课程 技术. 在有机化学中， 通过质子和碳13光谱进行结构分析。 FT-NMR表征产物的更高灵敏度将 在微型有机实验室中使用。 实验 将介绍，以提高学生对核磁共振的认识 应用. 强磁场与化学位移 将使用试剂来解析复合物的光谱 分子和光学立体异构体混合物。 发达 课程将提供各种实验， 举例说明和解释当前使用NMR技术， 核自旋退耦和核弛豫测量 在分子结构中。 有机反应 过渡金属配位化合物中的配体将是 通过碳-13观测进行监测。

This project will introduce the capabilities of 200 MHz Fourier transform nuclear magnetic resonance (FT-NMR) spectroscopy into our courses in organic chemistry and advanced experimental techniques. In organic chemistry the instrument will be used for structural analyses via proton and carbon-13 spectroscopy. The greater sensitivity of FT-NMR to characterize products will find use in the microscale organic laboratory. Experiments will be introduced to increase student awareness of NMR applications. The high magnetic field and chemical shift reagents will be utilized to resolve spectra of complex molecules and optical stereoisomer mixtures. In the advanced course a variety of experiments will be offered which illustrate and explain currently used NMR techniques such as nuclear spin decoupling and measurement of nuclear relaxation times within a molecular structure. Reactions of organic ligands in transition metal coordination compounds will be monitored via carbon-13 observation.