The Contribution of Variable Pressure Scanning Electron Microscopy (VPSEM) Coupled with Energy Dispersive X-ray (EDS) and Raman Spectroscopy (RS) to Anthropologically Oriented Arch

变压扫描电子显微镜 (VPSEM) 结合能量色散 X 射线 (EDS) 和拉曼光谱 (RS) 对人类学导向拱门的贡献

• 批准号: 0813649
• 负责人: Ioanna Kakoulli
• 金额: --
• 依托单位: University of California-Los Angeles
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 2008
• 资助国家: 美国
• 起止时间: 2008-07-01 至 2009-12-31
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=0813649&HistoricalAwards=false
• 关键词: Contribution; Variable; Pressure; Scanning; Electron

With National Science Foundation support the Laboratory of Materials Research in Archaeology and Cultural Heritage (a joint venture between the Cotsen Institute of Archaeology and the Materials Science and Engineering Department at UCLA) will acquire a state of the art Variable Pressure Scanning Electron Microscope (VPSEM) coupled with Energy Dispersive (EDS) and Raman Spectroscopy (RS) to foster cutting-edge research in integrated forensic bioanthropology and geoarchaeology. The combined capabilities of this instrument integrating imaging and morphological observations at nano length scale with elemental and molecular analysis of inorganic and organic materials provide a very powerful tool for the study of archaeological materials to answer important questions relating to production methods and material distribution reflecting the social structure and organization of ancient populations. The environmental capabilities of the VPSEM will allow archaeological artifacts to be analyzed non-invasively and without modification of their structure or chemistry. Archaeological materials that contain some moisture in their structure will be analyzed without risking dehydration and structural modifications. The versatile capabilities of this instrument will, undoubtedly, provide a new perspective and a novel approach to material characterization to answer anthropological questions regarding provenance of materials, production centers and intercultural and interregional relationships. A broad range of archaeological and cultural materials will be analyzed including ceramics, stone, basketry, textiles, botanical and biological remains, to support dating and provenance studies, the interpretation of environment change through time and environmentally-induced weathering and other changes. Two project-based examples of VPSEM/EDS/RS applications are: 1) the study of bioarcheological specimens from Pre-Columbian mummies in Chile to assist in the interpretation of the cultural and biological origins of the mid-valley prior to the Middle Horizon Period (AD 500-1000); 2) variability and sourcing of glaze-paint recipes of Ancestral Puebloan glazed-ceramics.Driven by newly established interdisciplinary research and education programs operating at the interface of science and archaeology, this instrument will be used by faculty and students from UCLA to facilitate teaching and multidisciplinary research in materials science based archaeology and to foster national and international collaborations with museums and universities. Research results will be disseminated through discussion groups, peer reviewed articles and the creation of databases that can be accessed by scholars and the broader archaeological community. The support from the National Science Foundation will also provide seed funding for the development of courses for graduate and undergraduate students on "technology applied to archaeological method and theory" and on "microscopy and microanalysis for anthropologically oriented archaeology". It will also assist at establishing further the outreach activities of the LMR focusing on K-12 students of unrepresented communities through interactive hands-on laboratory practical sessions and laboratory visits.

国家自然科学基金资助的考古与文化遗产材料研究实验室（科特森考古研究所和加州大学洛杉矶分校材料科学与工程系的合资企业）将获得最先进的变压扫描电子显微镜（VPSEM），结合能量色散（EDS）和拉曼光谱（RS），以促进切割-综合法医生物人类学和地质考古学的边缘研究。该仪器的综合能力将纳米尺度的成像和形态观察与无机和有机材料的元素和分子分析相结合，为考古材料的研究提供了一个非常强大的工具，以回答与反映古代人口社会结构和组织的生产方法和材料分布有关的重要问题。VPSEM的环境能力将允许考古文物进行非侵入性分析，而无需修改其结构或化学。在结构中含有一些水分的考古材料将被分析，而不会有脱水和结构改变的风险。这种仪器的多功能，无疑将提供一个新的视角和一种新的方法来描述材料，以回答人类学的问题，有关材料的来源，生产中心和跨文化和区域间的关系。将分析广泛的考古和文化材料，包括陶瓷，石头，编织物，纺织品，植物和生物遗迹，以支持测年和起源研究，通过时间和环境引起的风化和其他变化的环境变化的解释。VPSEM/EDS/RS应用的两个基于项目的例子是：1）研究智利前哥伦布时期木乃伊的生物考古标本，以帮助解释中地平线时期之前中谷的文化和生物起源（公元500-1000年）; 2）普韦布洛祖先釉彩配方的可变性和来源-陶瓷。在新建立的跨学科研究和教育计划的推动下，在科学和考古学的界面上运作，该仪器将被加州大学洛杉矶分校的教师和学生用于促进基于材料科学的考古学的教学和多学科研究，并培养国家以及与博物馆和大学的国际合作。研究成果将通过讨论小组、同行评审文章和建立可供学者和更广泛的考古界访问的数据库进行传播。国家科学基金会的支助还将提供种子资金，用于为研究生和本科生开设“应用于考古方法和理论的技术”和“面向人类学的考古学的显微镜和微量分析”课程。它还将通过互动式动手实验室实践课程和实验室参观，协助进一步建立LMR的外联活动，重点是无代表社区的K-12学生。