MRI: Acquisition of X-Ray Diffraction System

MRI：X 射线衍射系统的采集

• 批准号: 2215247
• 负责人: Wilfredo Otano
• 金额: $ 30.41万
• 依托单位: University of Puerto Rico Cayey
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 2022
• 资助国家: 美国
• 起止时间: 2022-09-01 至 2023-08-31
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=2215247&HistoricalAwards=false
• 关键词: MRI; Acquisition; Ray; Diffraction; System

This Major Research Instrumentation (MRI) program grant supports the acquisition of a state-of-the-art X-Ray Diffraction System (XRD) to advance research and educational activities in physics, chemistry, materials science, and engineering. Located in the southeast of the island, the Cayey campus of the University of Puerto Rico provides access to the XRD system to faculty and students from across the island. The XRD system enables over nine research groups to advance their research projects using diffraction techniques which are only available at this facility. Primary users include faculty from the University of Puerto Rico in the Mayaguez Campus, and the Ana G. Mendez University while researchers from UPR Ponce, Río Piedras, and Humacao campus also benefit as secondary users. The project promotes collaboration between different research groups, training for faculty and students, and educational activities. Training and workshops are offered to undergraduate students participating in research or taking courses that include the use of this instrumentation.The obtained high-resolution X-Ray diffraction system is ideal for the characterization of crystallinity in thin films, nanostructures, and low diffracting materials. The combination of the parallel beam optics, a channel-cut monochromator, and the goniometer’s triple-axis measurement capacity, allows for high-resolution measurements. The addition of an area detector allows for the study of crystal orientations, not only improving the information obtained for a particular crystal phase, but also providing information on the crystalline texture, defects, and crystalline size amongst others. This instrument enables the study of nanoparticles, multilayers, and thin films with nanometric morphologies. Furthermore, the high-temperature heating attachment and the texture, stress, and Rietveld plugins provide advanced techniques such as reciprocal space mapping, rocking curve, and pole figures measurements. Projects that benefit from this instrument include studies of multiferroic tunnel junctions, characterization of silver nanoparticles for surface-enhanced Raman spectroscopy, studies of zinc oxide for sensing harmful gases in the parts per billion range, investigations of defects in doped GaN, and the use of the XRD system in integrated undergraduate laboratory experiments including topics from different physics and chemistry sub-disciplines and a variety of instrumental techniques.This project is jointly funded by the NSF Office of Integrated Activities (OIA), and the Established Program to Stimulate Competitive Research (EPSCoR).This award reflects NSF's statutory mission and has been deemed worthy of support through evaluation using the Foundation's intellectual merit and broader impacts review criteria.

该主要研究仪器（MRI）项目拨款支持购买最先进的x射线衍射系统（XRD），以推进物理、化学、材料科学和工程方面的研究和教育活动。波多黎各大学Cayey校区位于该岛东南部，为全岛的教师和学生提供XRD系统的访问。XRD系统使超过9个研究小组能够使用仅在该设施可用的衍射技术推进他们的研究项目。主要用户包括波多黎各大学马亚圭斯校区和Ana G. Mendez大学的教师，而来自普遍定期审议庞塞、Río Piedras和Humacao校区的研究人员也作为次要用户受益。该项目促进了不同研究小组之间的合作、对教师和学生的培训以及教育活动。为参与研究或参加包括使用该仪器的课程的本科生提供培训和讲习班。所获得的高分辨率x射线衍射系统是表征薄膜，纳米结构和低衍射材料的结晶度的理想选择。平行光束光学，通道切割单色仪和测角仪的三轴测量能力的组合，允许高分辨率的测量。区域检测器的添加允许对晶体取向的研究，不仅改善了对特定晶体相的信息，而且还提供了关于晶体结构、缺陷和晶体尺寸等的信息。该仪器能够研究纳米颗粒、多层和具有纳米形貌的薄膜。此外，高温加热附件和纹理、应力和Rietveld插件提供了先进的技术，如互反空间映射、摇摆曲线和极形测量。受益于该仪器的项目包括多铁隧道结的研究、用于表面增强拉曼光谱的银纳米粒子的表征、用于探测十亿分之一范围内有害气体的氧化锌的研究、掺杂GaN的缺陷的研究，以及在综合本科实验室实验中使用XRD系统，包括来自不同物理和化学子学科的主题以及各种仪器技术。该项目由美国国家科学基金会综合活动办公室（OIA）和促进竞争性研究的既定计划（EPSCoR）共同资助。该奖项反映了美国国家科学基金会的法定使命，并通过使用基金会的知识价值和更广泛的影响审查标准进行评估，被认为值得支持。