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Synthesis of C-Nucleosides Related Oxetanocin

Synthesis of C-Nucleosides Related Oxetanocin
C-核苷相关的奥沙坦星的合成
批准号:
63870089
负责人:
YAMANAKA Hiroshi
金额:
$1.79万
依托单位:
依托单位国家:
日本
项目类别:
Grant-in-Aid for Developmental Scientific Research
财政年份:
1988
资助国家:
日本
项目状态:
已结题
起止时间:
1988 至 1989

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中文摘要
翻译
为了发展具有抗病毒活性的杂环化合物的化学,研究了与氧杂环霉素相关的核苷的合成。1)吡咯并嘧啶类化合物的闭环研究作为基础研究,建立了吡咯并[2,3-d]嘧啶和吡咯并[3,2-d]嘧啶类化合物的合成新方法。2)尿嘧啶型C-核苷的合成从5-溴-2,4-双(苄氧基)嘧啶开始,如下所示完成5-嘧啶基氧杂环丁烷糖的合成。3)脱氮嘌呤型核苷的合成基于第1部分中描述的结果,合成了以下无环嘌呤核苷。
英文摘要
In order to develop the chemistry of heterocyclic compounds having antiviral activities, synthesis of nucleosides relating to oxetanocin was investigated. 1) Ring-Closure to Pyrrolopyrimidines New methods for the synthesis of pyrrolo[2,3-d]pyrimidine and pyrrolo[3,2- d]pyrimidine derivatives was established as a basic investigation. 2) Synthesis of Uracil-Type C-Nucleoside Starting from 5-bromo-2,4-bis(benzyloxy)pyrimidine, the synthesis of the 5-pyrimidinyloxetanose was accomplished as shown below. 3) Synthesis of Deazapurine-Type Nucleosides On the basis of the results described in Section 1, the following acyclonucleosides was synthesized.
期刊论文(20)
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会议论文
Yoshinori Kondo: "Studies on Pyrimidine Derivatives.XLI.Palladium-Catalyzed Cross-Coupling Reaction of Halopyrimidines with Aryl-and Vinyltributylstannanes" Chemical & Pharmaceutical Bulletin. 37. 2814-2816 (1989)
Yoshinori Kondo:“嘧啶衍生物的研究。XLI.钯催化卤代嘧啶与芳基和乙烯基三丁基锡烷的交叉偶联反应”化学
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通讯作者:
Yuh-ichiro Ichikawa, Setsuko Niitsuma, Kuniki Kato, and Tomohisa Takita: "Preparation of trans-3-(Hydroxymethyl)-2-vinyloxetanocin via Allyloxycarbanion-mediated Carbon-Carbon Bond Formation in Allyl Glycidyl Ether" Journal of Chemical Society, Chemical C
Yuh-ichiro Ichikawa、Setsuko Niitsuma、Kuniki Kato 和 Tomohisa Takita:“通过烯丙氧基碳负离子介导的烯丙基缩水甘油醚中的碳-碳键形成制备反式 3-(羟甲基)-2-乙烯基氧杂环己烷”化学会杂志,化学 C
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Yuh-ichiro Ichikawa: "Preparation of trans-3-(Hydroxymethyl)-2-vinyloxetane via Allyoxycarbanion-mediated Carbon-Carbon Bond Formation in Allyl Glycidyl Ether" Journal of Chemical Society,Chemical Communication. 625-626 (1988)
Yuh-ichiro Ichikawa:“通过烯丙基缩水甘油醚中烯丙氧基碳负离子介导的碳-碳键形成制备反式-3-(羟甲基)-2-乙烯基氧杂环丁烷”《化学学会杂志》,《化学通讯》。
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