NMR SPECTROMETER

核磁共振波谱仪

• 批准号: 3522019
• 负责人: EDWIN VEDEJS
• 金额: $ 10.1万
• 依托单位: UNIVERSITY OF WISCONSIN-MADISON
• 依托单位国家: 美国
• 财政年份: 1993
• 资助国家: 美国
• 起止时间: 1993-09-01 至 1994-08-31
• 项目状态: 已结题
• 来源: https://reporter.nih.gov/project-details/3522019
• 关键词: biomedical automation; biomedical equipment purchase; biomedical equipment resource; computer network; computer program /software; computer system hardware; nuclear magnetic resonance spectroscopy; personal computers

The Department of Chemistry at the University of Wisconsin, Madison requests matching funds to purchase a Nuclear Magnetic Resonance (NMR) spectrometer to replace a ten year old 200 MHz NMR spectrometer used for routine high resolution NMR spectroscopy. The new spectrometer will operate at a field of 7.06 Tesla (300 MHz proton resonance); it will have both routine proton and carbon capabilities. An automatic sample changer will be added to the instrument to increase throughput of samples. To make the most effective use of the spectrometer the department also plans to upgrade the seven NMR data stations which are now used to carry out all of the off-line data processing. This new spectrometer is urgently needed in order to continue a number of research programs supported by the NIH. Although this equipment is located in the chemistry building, this facility serves the entire campus at the University of Wisconsin-Madison.

威斯康辛大学麦迪逊分校化学系

项目成果

Copper(I)/ABNO-catalyzed aerobic alcohol oxidation: alleviating steric and electronic constraints of Cu/TEMPO catalyst systems.

• DOI: 10.1021/ja409241h
• 发表时间: 2013-10-23
• 期刊: Journal of the American Chemical Society
• 影响因子: 15
• 作者: Steves JE;Stahl SS
• 通讯作者: Stahl SS

Synthesis and characterization of the 7-(4-aminomethyl-1H-1,2,3-triazol-1-yl) analogue of kabiramide C.

• DOI: 10.1021/np049670z
• 发表时间: 2005-02
• 期刊: Journal of natural products
• 影响因子: 5.1
• 作者: Chutima Petchprayoon;K. Suwanborirux;Reagan L. Miller;T. Sakata;G. Marriott

Method for Small-Scale Production of Deuterochloroform.

小规模生产氘代氯仿的方法。

• DOI: 10.1021/acs.joc.8b01018
• 发表时间: 2018
• 期刊: The Journal of organic chemistry
• 作者: Tansukawat,NathaD;See,AlyaaE;Jiranuntarat,Sadudee;Corbin,JoshuaR;Schomaker,JenniferM
• 通讯作者: Schomaker,JenniferM

Copper-catalyzed recycling of halogen activating groups via 1,3-halogen migration.

• DOI: 10.1021/ja306446m
• 发表时间: 2012-10-03
• 期刊: Journal of the American Chemical Society
• 影响因子: 15
• 作者: Grigg RD;Van Hoveln R;Schomaker JM
• 通讯作者: Schomaker JM

[2+2] cycloadditions by oxidative visible light photocatalysis.

• DOI: 10.1021/ja103934y
• 发表时间: 2010-06-30
• 期刊: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
• 影响因子: 15
• 作者: Ischay, Michael A.;Lu, Zhan;Yoon, Tehshik P.
• 通讯作者: Yoon, Tehshik P.