The Preparation of Levulinic Acid by Acid-catalyzed Hydrolysis of Bamboo Shoot Shell in the Presence of Acidic Ionic Liquid Using the Box-Behnken Design
The Preparation of Levulinic Acid by Acid-catalyzed Hydrolysis of Bamboo Shoot Shell in the Presence of Acidic Ionic Liquid Using the Box-Behnken Design
复制标题
采用 Box-Behnken 设计在酸性离子液体存在下酸催化水解竹笋壳制备乙酰丙酸
DOI：
10.1080/15567036.2010.529560
复制
发表时间：
2013-08
期刊：
影响因子：
--
通讯作者：
Vittayapadung S.
中科院分区：
文献类型：
--
作者：
Zhang Youzuo;Wang Yunxiang;Lin Lin;Vittayapadung S.
采用Box-Behnken设计对离子液体水解竹笋壳制备乙酰丙酸进行了研究。建立了一个回归模型来描述自变量及其交互作用对乙酰丙酸产率的影响。R型离子液体和反应时间的相关系数P值分别为<0.0001和0.005，表明这两种影响是显著的。二阶模型的相关系数测定（R2 = 96.18%）表明，实验数据和模型数据之间得到了良好的协议。在最佳条件下进行了乙酰丙酸收率的验证试验，乙酰丙酸收率为38.2%，与预测值基本一致。
Studies on the hydrolysis of bamboo shoot shell to levulinic acid with ionic liquid using Box-Behnken design were carried out. A regression model was developed to describe the effects of independent variables and their interactions on levulinic acid yield. The P-value of coefficient for R ionic liquid and reaction time were <0.0001 and 0.005, respectively, suggesting that the two effects were significant. The coefficient determination (R 2 = 96.18%) for the second-order model showed that good agreement between the experimental and modeled data was obtained. Confirmatory tests, with a levulinic acid yield of 38.2%, were obtained under the optimum conditions, which closely agreed with the predicted value.
登录
查看更多内容
DOI：
10.5860/choice.36-0035
发表时间：
2001
期刊：
--
影响因子：
--
作者：
H. Zoebelein
通讯作者：
H. Zoebelein
影响因子：
3.9
作者：
Girisuta, B.;Janssen, L. P. B. M.;Heeres, H. J.
通讯作者：
Heeres, H. J.
影响因子：
9.8
作者：
Huddleston, JG;Visser, AE;Rogers, RD
通讯作者：
Rogers, RD
影响因子：
13.2
作者：
Bozell, JJ;Moens, L;Jarnefeld, JL
通讯作者：
Jarnefeld, JL
影响因子：
3.9
作者：
Muralidhar, RV;Chirumamila, RR;Nigam, P
通讯作者：
Nigam, P