SBIR Phase II: Coupled High Performance Liquid Chromatography with Fourier Transform Infrared Spectroscopy Instrumentation for the Characterization of Polymers

SBIR 第二阶段：高效液相色谱与傅里叶变换红外光谱仪器联用，用于聚合物表征

• 批准号: 9501303
• 负责人: James Dwyer
• 金额: $ 14.97万
• 依托单位: Lab Connections, Inc.
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 1997
• 资助国家: 美国
• 起止时间: 1997-07-15 至 1998-06-30
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=9501303&HistoricalAwards=false
• 关键词: SBIR; Phase; II; Coupled; Performance

9501303 Dwyer This Small Business Innovation Research Phase II project will significantly improve hyphenated Liquid Chromatography/Infrared (LC/IR) Spectroscopy technology for use in polymer characterization. This methodology provides a marked advance over conventional chromatography/IR spectroscopic analytic methods. Phase I research successfully developed a prototype for a wide variety of polymer applications. The Phase II research plan is divided into four parts: (1) define limits of the system, including quantitative analysis, and examination of artifacts; (2) expand the list of applications: test additional copolymer systems, as well as blends and alloys; (3) modify system design to provide automated multi-sample analysis; and (4) develop 3D/IR software to link with commercial chromatography software packages, and to provide additional modes of data analysis. The combined capacity of the hardware/software represents a quantum advance in capability for polymer characterization. The results of this study will expand the commercial market to polymer scientists working on a wide range of applications from research to manufacturing and quality control.

这个小型企业创新研究二期项目将显著改进用于聚合物表征的联用液相色谱/红外（LC/IR）光谱技术。这种方法比传统的色谱/红外光谱分析方法有了显著的进步。第一阶段的研究成功地开发了一种广泛应用于聚合物的原型。第二阶段的研究计划分为四个部分：(1)确定系统的范围，包括定量分析和人工制品的检查；(2)扩大应用范围：测试额外的共聚物体系，以及共混物和合金；(3)修改系统设计，提供自动化多样品分析；(4)开发3D/IR软件，与商业色谱软件包链接，并提供额外的数据分析模式。硬件/软件的组合能力代表了聚合物表征能力的量子进步。这项研究的结果将把商业市场扩大到从事从研究到制造和质量控制等广泛应用的聚合物科学家。