X-Ray Photoelectron Spectrometer

化学研究所、材料科学研究所和微型生产技术研究所的工作组要求提供X射线光电子能谱仪。该研究设备将用于各种研究项目：-作为物理化学和电化学研究所功能纳米结构研究的一部分，用于结构-性能相关性的研究，即1。表面化学和深度分布的详细表征以及尺寸、形状和组成受控的半导体和金属纳米颗粒以及磁性纳米颗粒及其微结构的局部元素分布的测定2。测定半导体纳米颗粒的导带和价带结构（也是温度相关的测量），特别是量子点、纳米颗粒网络、纳米棒和来自胶体化学合成的2D半导体纳米结构。这种表征在来自上述颗粒的组件上进行3.纳米结构膜的表面质量和化学组成的深度分布的测定（例如基于MXene的膜，基于金属有机骨架连接的混合基质膜）和各种热电材料，作为无机材料研究的一部分，在无机化学研究所中详细分析了以下结构：1.研究植入物相关或定向给药系统（多孔无机和混合材料）：测试纳米颗粒表面和植入物表面的成功化学改性（例如二氧化硅，陶瓷，二氧化钛上的膦酸盐附着，用硫醇装饰贵金属表面等）以及电化学沉积材料2。研究上述多孔材料在上微米尺度上的药物释放和结合的空间分辨率，用于植入研究，以改善其功能3。纳米多孔光学、光电和电子材料的计算电子和光学性质的比较（主要是金属-有机框架连接）与来自X射线和UV范围内的光电子能谱和逆光电子能谱的实验可用数据-作为材料科学研究所研究的一部分，金属/金属和金属/陶瓷复合材料中的金属结构和功能材料以及界面的详细表征-作为传感器研究的一部分，在微型生产技术研究所制造的致动器和其他功能性微结构和系统，用于界面的化学分析和确定各种材料的材料损伤和深度分布，例如通过各种生产技术中的磨损机制

An X-ray photoelectron spectrometer is requested by working groups from the chemical institutes, the institute of materials science and the institute of micro production technology. The research device is to be used in various research projects:- as part of research on functional nanostructures at the Institute of Physical Chemistry and Electrochemistry in the investigation of structure-property correlations, namely1. Detailed characterization of surface chemistry and depth profile as well as determination of the local elementary distributions of size, shape and composition controlled semiconductor and metal nanoparticles as well as magnetic nanoparticles and their assemblies2. Determination of the conduction and valence band structure (also temperature-dependent measurements) of semiconductor nanoparticles, in particular of quantum dots, nanoparticle networks, nanorods and of 2D semiconductor nanostructures from colloid-chemical syntheses. Such characterizations are carried out on assemblies from the above mentioned particles3.Determination of the surface quality and depth profile of the chemical composition of nanostructured membranes (e.g. MXene-based membranes, mixed matrix membranes based on metal organic framework connections) and of various thermoelectric materials- as part of research on inorganic materials at the Institute of Inorganic Chemistry in the detailed analysis of the following structures:1. Investigations on implant-associated or -directed drug delivery systems (porous inorganic and hybrid materials): Testing the successful chemical modification of the surface of nanoparticles and implant surfaces (e.g. on silica, ceramics, phosphonate attachment on titanium dioxide, decoration of precious metal surfaces with thiols etc.) as well as electrochemically deposited materials2. Investigation of the spatial resolution of the drug release and binding on the upper micron scale on the above-mentioned porous materials for implant research to improve their functionality3. Comparison of the calculated electronic and optical properties of nanoporous optical, optoelectronic and electronic materials (mainly metal-organic framework connections) with experimentally available data from photoelectron spectroscopy in the X-ray and UV range and inverse photoelectron spectroscopy- as part of research at the Institute of Materials Science, the detailed characterization of metallic structural and functional materials and interfaces in metal/metal and metal/ceramic composites- as part of the research on sensors, actuators and other functional microstructures and systems manufactured at the Institute of Micro Production Technology for the chemical analysis of interfaces and the determination of material damage and depth profiles of various materials, for example through wear mechanisms in various production techniques