Determination of the tilt and twist angles of curved GaN layers by high-resolution x-ray diffraction

Determination of the tilt and twist angles of curved GaN layers by high-resolution x-ray diffraction
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通过高分辨率 X 射线衍射测定弯曲 GaN 层的倾斜角和扭转角

DOI:
10.1088/0268-1242/24/12/125007
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发表时间:
2009-12
影响因子:
1.9
通讯作者:
--
中科院分区:
工程技术4区
文献类型:
--
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用x射线摇摆曲线的半最大值全宽度(FWHM)作为确定氮化镓层倾斜和扭转角的参数。然而,当GaN脱毛层的厚度达到几微米时,由于曲率引起的峰展宽变得不可忽略。本文系统地研究了利用(0 0 l), l = 2,4,6, XRC来最小化晶圆曲率的影响。提出了在Williamson-Hall图不适合的情况下确定GaN弯曲层倾斜角度的方法。结果表明,(0 0 6)XRC-FWHM对于制备半径曲率r小于3.5 m的高质量GaN层具有显著的优势。此外,还提出了一种获得可靠倾斜角度的外推方法,对于r < 2 m的晶体,与(0 0 6)XRC-FWHM相比,计算误差可提高10%。在歪斜几何中,我们证明了(2 0 4)XRC-FWHM得到的扭转角与明显弯曲样品的掠入射面内衍射(IP-GID)方法得到的扭转角是一致的。
The full-width at half-maximum (FWHM) of an x-ray rocking curve (XRC) has been used as a parameter to determine the tilt and twist angles of GaN layers. Nevertheless, when the thickness of GaN epilayer reaches several microns, the peak broadening due to curvature becomes non-negligible. In this paper, using the (0 0 l), l = 2, 4, 6, XRC to minimize the effects of wafer curvature was studied systematically. Also the method to determine the tilt angle of a curved GaN layer was proposed while the Williamson–Hall plot was unsuitable. It was found that the (0 0 6) XRC-FWHM had a significant advantage for high-quality GaN layers with the radius curvature of r less than 3.5 m. Furthermore, an extrapolating method of gaining a reliable tilt angle has also been proposed, with which the calculated error can be improved by 10% for r < 2 m crystals compared with the (0 0 6) XRC-FWHM. In skew geometry, we have demonstrated that the twist angles deriving from the (2 0 4) XRC-FWHM are in accord with those from the grazing incidence in-plane diffraction (IP-GID) method for significantly curved samples.
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影响因子: 3.2
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