Preparation and optimization of freestanding GaN using low-temperature GaN layer

Preparation and optimization of freestanding GaN using low-temperature GaN layer
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使用低温GaN层制备和优化独立式GaN

DOI:
10.1007/s11706-019-0466-z
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发表时间:
2019-09
影响因子:
2.7
通讯作者:
Hu Haixiao
Hu Haixiao
中科院分区:
材料科学3区
文献类型:
--
作者:
Tian Yuan;Shao Yongliang;Hao Xiaopeng;Wu Yongzhong;Zhang Lei;Dai Yuanbin;Huo Qin;Zhang Baoguo;Hu Haixiao

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本文提出了一种利用低温GaN层获得自支撑GaN的方法。为了获得多孔结构和增加结晶度,LT-GaN层在高温下退火。分析了不同厚度和不同退火温度的LT-GaN层退火前后的形貌。通过对不同LT-GaN层制备GaN薄膜的比较,获得了最佳的LT-GaN工艺。HRXRD和拉曼结果表明,在1090 °C退火的800 nm LT-GaN层上生长的GaN具有良好的晶体质量和较小的应力。在冷却之后,GaN膜成功地与衬底分离。对该方法的自分离机理进行了探讨。利用截面EBSD成像测量研究了低温缓冲层对晶体质量的改善和应力消除的作用。通过PL测量还确定了所获得的自支撑GaN膜的光学性质。
In this work, a method to acquire freestanding GaN by using low temperature (LT)-GaN layer was put forward. To obtain porous structure and increase the crystallinity, LT-GaN layers were annealed at high temperature. The morphology of LT-GaN layers with different thickness and annealing temperature before and after annealing was analyzed. Comparison of GaN films using different LT-GaN layers was made to acquire optimal LT-GaN process. According to HRXRD and Raman results, GaN grown on 800 nm LT-GaN layer which was annealed at 1090 °C has good crystal quality and small stress. The GaN film was successfully separated from the substrate after cooling down. The self-separation mechanism of this method was discussed. Cross-sectional EBSD mapping measurements were carried out to investigate the effect of LT-buffer layer on improvement of crystal quality and stress relief. The optical property of the obtained freestanding GaN film was also determined by PL measurement.
DOI: 10.1063/1.3195684
发表时间: 2009-08-03
影响因子: 4
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