Fourier Transform Nuclear Magnetic Resonance Spectrometry in the Chemistry Curriculum

化学课程中的傅里叶变换核磁共振波谱分析

• 批准号: 9250494
• 负责人: Richard Watkins
• 金额: $ 8.87万
• 依托单位: Carroll University
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 1992
• 资助国家: 美国
• 起止时间: 1992-06-01 至 1995-11-30
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=9250494&HistoricalAwards=false
• 关键词: Fourier; Transform; Nuclear; Magnetic; Resonance

The Chemistry Department has identified laboratory improvement guidelines including the needs: to incorporate work using smaller and more complex samples, to emphasize real world chemistry, to use state-of-the-art instrumentation, to increase laboratory efficiency so that more experimental work can be done, and to increase the understanding of chemical health and safety. Acquisition of a 200 MHz FT-NMR Spectrometer with a variable temperature module will enhance all but the last of those principles in five of our upper division courses. Specific improvements include enhanced proton analysis, a new capability for 13C analysis, the computer controlled acquisition and processing of data, application of FT-NMR analysis to small samples, determination of kinetic and thermodynamic parameters, and special pulse sequences for simplification of complex spectra. In addition, the instrument will increase the range of projects available to undergraduates doing research.

化学系已确定实验室改进 准则，包括需要： 更小和更复杂的样本，以强调真实的世界 使用最先进的仪器， 实验室效率，以便更多的实验工作， 完成，并增加对化学品健康的了解， 安全为代价的 购买一台200 MHz FT-NMR光谱仪 可变温度模块将提高所有，但最后的 这些原则在我们的五个高年级课程。 具体的改进包括增强的质子分析，一个新的 13 C分析能力，计算机控制采集 和数据处理，应用FT-NMR分析小 样品，动力学和热力学参数的测定， 和特殊的脉冲序列，用于简化复杂的 谱 此外，该仪器将增加射程 的项目提供给本科生做研究。