Development of Titanium Catalyzed Reactions for Multicomponent Couplings and Heterocyclic Synthesis

钛催化多组分偶联和杂环合成反应的进展

基本信息

  • 批准号:
    0715556
  • 负责人:
  • 金额:
    $ 39.3万
  • 依托单位:
  • 依托单位国家:
    美国
  • 项目类别:
    Continuing Grant
  • 财政年份:
    2007
  • 资助国家:
    美国
  • 起止时间:
    2007-08-01 至 2010-07-31
  • 项目状态:
    已结题

项目摘要

Professor Aaron Odom of Michigan State University is supported by the Inorganic, Bioinorganic and Organometallic Chemistry program to develop catalytic C-N bond forming reactions, particularly those that construct frameworks relevant to heterocyclic synthesis. The central reactions being explored are hydroamination and hydrohydrazination of olefins and alkynes using titanium catalysts with pyrrolyl based ancillary ligands. New protocols are also being developed for three component coupling reactions that bring together hydrazine, isonitrile and alkyne reagents.Formation of heterocyclic products via atom efficient coupling methodologies provides the foundation for this project that features the addition of either an amine or hydrazine to an alkene or an alkyne. The broader impacts of this project also include training students in both inorganic and organic mechanistic chemistry and in teaching students sophisticated experimental techniques encompassing multinuclear NMR, kinetics, and x-ray diffraction.
密歇根州立大学的Aaron Odom教授得到了无机,生物无机和有机化学计划的支持,以开发催化C-N键形成反应,特别是那些构建与杂环合成相关的框架的反应。正在探索的中心反应是使用钛催化剂与吡咯基辅助配体的烯烃和炔的氢胺化和氢肼化。同时,还在开发新的三组分偶联反应方案,将肼、异腈和炔试剂结合在一起。通过原子有效偶联方法形成杂环产物为该项目提供了基础,该项目的特点是将胺或肼加成到烯烃或炔上。 该项目的更广泛的影响还包括培养学生在无机和有机机械化学和教学学生复杂的实验技术,包括多核NMR,动力学和X射线衍射。

项目成果

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Aaron Odom其他文献

Aaron Odom的其他文献

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{{ truncateString('Aaron Odom', 18)}}的其他基金

Discovering Design Criteria in Early Transition Metal Catalysis
发现早期过渡金属催化的设计标准
  • 批准号:
    2247064
  • 财政年份:
    2023
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Continuing Grant
CAS: Developing Methods for Reaction Modeling to Tune Catalysts for Substrate Variability
CAS:开发反应建模方法来调整催化剂的底物变化
  • 批准号:
    1953254
  • 财政年份:
    2020
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Standard Grant
MRI: Acquisition of a Duo Source Single Crystal X-ray Diffractometer for the Center for X-ray Crystallographic Research
MRI:为 X 射线晶体学研究中心购置双源单晶 X 射线衍射仪
  • 批准号:
    1919565
  • 财政年份:
    2019
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Standard Grant
SusChEM: Tools for the Development of High-Valent Transition Metal Catalysts
SusChEM:开发高价过渡金属催化剂的工具
  • 批准号:
    1562140
  • 财政年份:
    2016
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Standard Grant
SusChEM: Development and Applications of Ligand Donor Parameters for High Valent Transition Metal Systems
SusChEM:高价过渡金属体系配体供体参数的开发和应用
  • 批准号:
    1265738
  • 财政年份:
    2013
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Standard Grant
Development of Titanium Catalysts and Multicomponent Coupling Strategies Applicable to Heterocyclic Synthesis
适用于杂环合成的钛催化剂和多组分偶联策略的开发
  • 批准号:
    1012537
  • 财政年份:
    2010
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Standard Grant
Titanium catalyzed multi-component coupling strategies based on hydroamination of alkynes
基于炔烃加氢胺化的钛催化多组分偶联策略
  • 批准号:
    0350762
  • 财政年份:
    2004
  • 资助金额:
    $ 39.3万
  • 项目类别:
    Continuing Grant

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