Developement of in situ structural analyzes of bonding between different materials

不同材料之间粘合的原位结构分析的发展

• 批准号: 06555209
• 负责人: KIZUKA Tokushi
• 金额: $ 2.24万
• 依托单位: Nagoya University
• 依托单位国家: 日本
• 项目类别: Grant-in-Aid for Scientific Research (B)
• 财政年份: 1994
• 资助国家: 日本
• 起止时间: 1994 至 1996
• 项目状态: 已结题
• 来源: https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-06555209/
• 关键词: bonding; Transmission electron microscopy; hetero bonding; in situ analysis; atomic resolution; 高分解能透過電子顕微鏡; 電子線加工

Atomic scale solid state direct bonding in time-resolved high-resolution transmission electron microscopy was realized by using the piezodriven specimen holder. The structural variations of atomic arrangements in approach, contact, bonding and separation processes between two gold tips were observed at atomic scale. It was found that the nanometer-sized gold tips contact spontaneously when the tips approach at the critical distance corresponding to a few atomic distance underi intense electron irradiation. The crystallographic boundary forms after the contact. A few layrs near the surfaces and bonding-boundaries are responsible for the bonding and separation processes. New kinds of atomic scale mechanical tests such as the friction test, the compressing, tensile and shear deformation tests were proposed.

利用压电驱动样品保持器实现了时间分辨高分辨透射电镜中原子尺度的固态直接键合。在原子尺度上观察了两个金针尖在接近、接触、键合和分离过程中原子排列的结构变化。结果表明，在强电子辐照下，纳米金针尖在几个原子距离的临界距离处发生自发接触。晶体学边界在接触之后形成。界面附近的一些层和键合边界负责键合和分离过程。提出了摩擦试验、压缩、拉伸和剪切变形试验等新的原子尺度力学试验方法。

项目成果

T.Kizuka et al.: "Critical grain size for structural transformation in vacuum-deposited molybdenum films" Surf.Rev.Lett.3. 1181-1185 (1996)

T.Kizuka 等人：“真空沉积钼薄膜结构转变的临界晶粒尺寸”Surf.Rev.Lett.3。

T.Kizuka: "Time-resolved atomic observation of fragmentation of gold clusters by high-resolution electron microscopy" Surf.Rev.Lett.3. 1187-1190 (1996)

T.Kizuka：“通过高分辨率电子显微镜对金簇碎片进行时间分辨原子观察”Surf.Rev.Lett.3。

T.Kizuka et al.: "Structure and hardness of nanocrystalline silver" Journal of Materials Science. (in print). (1996)

T.Kizuka 等人：“纳米晶银的结构和硬度”材料科学杂志。

T.Kizuka: "Cross sectional high-resolution transmission electron microscopy of atomic scale contact and non-contact type scanning on gold surfaces" Phys.Rev.B. (in print). (1997)

T.Kizuka：“金表面原子级接触和非接触式扫描的横截面高分辨率透射电子显微镜”Phys.Rev.B。

T.Kizuka: "Time-resolved high-resolution electron microscopy of solid state direct bonding of gold and zinc oxide nanocrystallites" Appl.Phys.Lett.(in print). (1997)

T.Kizuka：“金和氧化锌纳米微晶固态直接键合的时间分辨高分辨率电子显微镜”Appl.Phys.Lett.（印刷中）。