Development of a new synthesis method for functional materials using liquid-liquid biphasic systems

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Inorganic synthesis was carried out using immiscible liquid-liquid biphasic systems under ambient pressure at moderate temperatures. Hybrid materials intercalated with organic acid ions were obtained for hydroxide compounds including transition metal or rare-earth metal elements. By dissolving different metal ions in organic and aqueous solutions, complex metal oxides could be formed through reactions at the liquid-liquid interface. Various materials thus obtained were evaluated as functional materials such as phosphors and electrodes of dye-sensitized solar cells.