An Inert Atmosphere Glove Box for Organoboron Materials Chemistry

用于有机硼材料化学的惰性气氛手套箱

• 批准号: 472543-2015
• 负责人: Wang, Suning
• 金额: $ 4.09万
• 依托单位: Queen's University
• 依托单位国家: 加拿大
• 项目类别: Research Tools and Instruments - Category 1 (<$150,000)
• 财政年份: 2014
• 资助国家: 加拿大
• 起止时间: 2014-01-01 至 2015-12-31
• 项目状态: 已结题
• 来源: https://www.nserc-crsng.gc.ca/ase-oro/Details-Detailles_eng.asp?id=564781
• 关键词: Inert; Atmosphere; Glove; Box; Organoboron

An inert atmosphere glove box is a standard and indispensible equipment for research in inorganic and organometallic chemistry. The primary function of a dry box in our laboratory is for the storage/transferring of air and moisture sensitive compounds and the preparation of oxygen-free samples for the study of luminescence, photochromic switching and photoelimination properties of organoboron compounds and metal complexes. Because the photochemistry work requires a box that is free of halogenated solvent or reagents, our research requires two dedicated glove boxes, one for work that needs halogenated solvent/reagent free conditions and the other for all work that can tolerate or require the use of halogenated solvents or reagents.

惰性气氛手套箱是无机化学和有机金属化学研究中不可缺少的标准设备。我们实验室的干燥箱的主要功能是储存/转移对空气和水分敏感的化合物，并制备无氧样品，用于研究有机硼化合物和金属配合物的发光、光致变色开关和光消除特性。由于光化学工作需要一个无卤化溶剂或试剂的盒子，我们的研究需要两个专用手套箱，一个用于需要无卤化溶剂/试剂条件的工作，另一个用于所有可以容忍或需要使用卤化溶剂或试剂的工作。