Acquisition of a High Field NMR Spectrometer, and its Integration into the Chemistry Curriculum

购买高场核磁共振波谱仪并将其纳入化学课程

• 批准号: 8852500
• 负责人: John E. Hancock
• 金额: $ 10万
• 依托单位: Reed College
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 1988
• 资助国家: 美国
• 起止时间: 1988-06-01 至 1990-11-30
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=8852500&HistoricalAwards=false
• 关键词: Acquisition; Field; NMR; Spectrometer; its

The chemistry curriculum is being upgraded with the acquisition of a Bruker AC-E 250 MHz NMR spectrometer with a special probe unit allowing detection of resonances from proton, carbon-13, fluorine-19 and phosphorus-31 nuclei under (switchable) computer control. The analytical capability is being extended with the ability to analyze all four nuclei and the data is being processed via a computer. The present laboratory curriculum is being extended with the introduction of new NMR experiments in six courses and with the ability to do 2D analysis of spectral data and appropriate double resonance and pulse techniques in senior thesis research. Students are running spectra on a user-friendly instrument in introductory organic and inorganic. Introductory organic is being converted to microscale syntheses and analyses with the increased sensitivity of the instrument. Senior thesis research is being facilitated with the new capability. The grantee is more than matching the award from non-Federal sources.

化学课程正在升级， Bruker AC-E 250 MHz NMR光谱仪，配有特殊探头单元， 探测质子、碳-13、氟-19和 磷-31核在（可切换的）计算机控制下。 的 分析能力正在扩展到分析所有 四个原子核，数据正在通过计算机进行处理。 的 目前的实验室课程正在扩大， 新的NMR实验在六门课程，并有能力做2D 分析光谱数据和适当的双共振和脉冲 高级论文研究的技巧。 学生们正在一个用户友好的仪器上运行光谱， 介绍有机和无机。 有机食品的介绍 转化为微型合成和分析， 仪器的灵敏度。 毕业论文研究正在 以新的能力来推动。 受赠人是超过匹配的奖励从非联邦来源。