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Development of a tritium compatible mass spectrometer.

Development of a tritium compatible mass spectrometer.
开发氚兼容质谱仪。
批准号:
61880019
负责人:
WATANABE Kuniaki
金额:
$6.91万
依托单位:
依托单位国家:
日本
项目类别:
Grant-in-Aid for Developmental Scientific Research
财政年份:
1986
资助国家:
日本
项目状态:
已结题
起止时间:
1986 至 1987

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中文摘要
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英文摘要
Tritium exposure gives rise to considerable increase in the noise of mass spectrometers. To avoid this imparirment and apply the mass spectrometer to tritium handling system for D-T burning fusion devices, we developed a tritium compatible quadrupole mass spectrometer equipped with tritium decontamination devices< Possible parts of the mass spectrometer were coated with gold to reduce the adsorption of tritium.It was observed that the noise level and width of the mass spectrometer increased with tritium exposure: namely, the noise level and width increased to 1E-9 and 5E-11 Amp., respectively, owing to cumulative tritium exposure of 0.1 Torr.sec. The increase in the noise level was about 100 times and that in the width was about 30 times of the initial one. It was confirmed that the increase in the noised due to the tritium adsorbed on the surfaces of inner wall of the vacuum system, quadrupole and detector itself: the tritium in gasphase playd only a minor role. The noise level and width could not be effectivly reduced by simple evacuation at room temperature. On the other hand, it was revealed that photon irradiation by halogen lamp caused to reduce both of the noise level and width to 2E-10 and 1.5E-11 Amp., respectively. They were about 1/15 or those of a conventional quadrupole mass spec- trometer after decontamination with similar procedures. The photon irradiation by mercury lamp acted similarly. The decontamination is not due to thermal effect but to photon induced desorption. These results indicate the mass spectrometer developed in the present study is compatible to carrier free tritium because the tritium contamination can be removed in-situ by photon irradiation to reduce the nose of the mass speqtrometer, although the improvement of the pumpling system and photon irradiation device should be required.
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会议论文
H.Miyake;K.Ichimura;M.Matsuyama;K.Ashida;K.Watanabe;S.Nakamura;and T.Hayashi.: Ann.Rept.Tritium Res.Center,Toyama Univ.
H.Miyake;K.Ichimura;M.Matsuyama;K.Ashida;K.Watanabe;S.Nakamura;和T.Hayashi.:富山大学Ann.Rept.氚研究中心。
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Absorption of Hydrogen Isotopes by Vanadium-based Low Activation Materials
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  • 项目类别:
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  • 资助金额:
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  • 财政年份:
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Analysis on the character evolution in Australian Gnaphalieae based on molecular phylogenetic tree.
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