Glovebox for synthesis and handling of air-sensitive materials for solid-state NMR studies

需要一个带气体净化系统、前厅和真空泵的惰性气氛手套箱。我们需要手套盒来制备和处理固体化合物，以便通过核磁共振(核磁共振)光谱进行研究。核磁共振是了解化合物结构和动力学的最通用和最有用的技术之一。手套盒是制备和操作与水分或氧气发生反应的化合物所必需的。这种化学物质在空气中不容易处理。手套盒提供惰性气氛(干燥的氩气或氮气)，因此可以轻松、安全地合成和研究活性化合物。例如，我们的目标是通过核磁共振光谱研究无机材料和重要催化剂中的钴-59核，而手套盒将使我们能够制备这些空气敏感材料。所需设备将极大地增加学生和博士后培训机会，特别是将在2009年立即使三名新的“高素质人员”受训人员受益。

An inert atmosphere glovebox with accompanying gas purification system, antechamber, and vacuum pump are requested. We require the glovebox to prepare and handle solid compounds to be studied by nuclear magnetic resonance (NMR) spectroscopy. NMR is one of the most versatile and useful techniques for learning about the structure and dynamics of chemical compounds. The glovebox is required for the preparation and manipulation of chemical compounds which react with moisture or oxygen. Such chemicals cannot be easily handled in air. The glovebox provides an inert atmosphere (dry argon or nitrogen gas) so that reactive compounds can easily and safely be synthesized and studied. For example, we are aiming to study cobalt-59 nuclei in inorganic materials and important catalysts by NMR spectroscopy, and the glovebox will enable us to prepare these air-sensitive materials. The requested equipment will greatly enhance student and postdoctoral training opportunities, and in particular will immediately benefit three new 'highly-qualified personnel' trainees in 2009.