Integration of Fourier Transform Infrared Spectrophotometry Into the Chemistry Curriculum

将傅里叶变换红外分光光度法融入化学课程

• 批准号: 9250468
• 负责人: Arthur Serianz
• 金额: $ 1.41万
• 依托单位: Saint Ambrose University
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 1992
• 资助国家: 美国
• 起止时间: 1992-07-15 至 1994-12-31
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=9250468&HistoricalAwards=false
• 关键词: Integration; Fourier; Transform; Infrared; Spectrophotometry

The Departments of Chemistry and Biology are purchasing a Fourier Transform infrared spectrometer (FTIR) for use in chemically oriented instruction in both departments. Students learn the use of computer controlled FTIR spectrophotometry for the elucidation of organic structures as well as data manipulation and analysis. The high sensitivity and analysis speed of the FTIR allow use for a greater variety of experiments than was possible with prior instruments. The computer search capabilities provide students with an understanding of the identification process inherent in infrared analysis and demonstrate the usefulness of computer database interfacing to instruments. In the organic chemistry laboratory, students use the instrument to identify the key chemical compounds involved in the multi-step synthesis of lidocaine from 2,6-dimethylnitrobenzene. In the instrumental analysis course, students study both the theoretical and practical aspects of FTIR. In the physical chemistry course, an experiment is performed to study the rotational fine structure of the infrared vibrational spectra of hydrogen chloride and deuterium chloride. In addition, a general education course in introductory chemistry for non-majors provides students with experiences in FTIR analysis involving such procedures as the purification of aspirin.

化学系和生物系正在购买 傅里叶变换红外光谱仪（FTIR），用于 化学导向教学在两个部门。 学生 学习使用计算机控制FTIR分光光度法， 对有机结构和数据的解释 操作和分析。 高灵敏度和分析 傅里叶变换红外光谱仪的速度允许用于更大范围的 实验比以前的仪器可能。 的 计算机搜索功能为学生提供了一个 对识别过程固有的理解， 红外分析和演示计算机的实用性 数据库与仪器接口。 有机化学 实验室，学生使用仪器识别钥匙 涉及多步合成的化合物 利多卡因是从2，6-二甲基硝基苯中提取的 在器乐 分析课程，学生学习理论和 FTIR的实用方面。 在物理化学课程中， 进行了实验研究， 氢的红外振动光谱结构 氯化物和氯化氘。 此外，一名将军 公共基础化学教育课程 为学生提供FTIR分析的经验，包括 例如阿司匹林的纯化。