A Regional NMR Training Cooperative with a Virtual Impact

具有虚拟影响力的区域核磁共振培训合作社

• 批准号: 0310861
• 负责人: Alline Somlai
• 金额: --
• 依托单位: Delta State University
• 依托单位国家: 美国
• 项目类别: Standard Grant
• 财政年份: 2003
• 资助国家: 美国
• 起止时间: 2003-08-01 至 2009-01-31
• 项目状态: 已结题
• 来源: https://www.nsf.gov/awardsearch/showAward?AWD_ID=0310861&HistoricalAwards=false
• 关键词: Regional; NMR; Training; Cooperative; Virtual

Chemistry (12) At Delta State University we are creating and developing a regional cooperative NMR facility by adapting and implementing a system developed at Rider University. This facility serves our institution, Coahoma Community College, Mississippi Delta Community College and the wider community in the region. Our overarching goal is to incorporate modern 1-D and 2-D FT-NMR spectroscopy throughout the undergraduate chemistry curricula at DSU, CCC and MDCC. To achieve our goal, we are adapting a series of experiments primarily from the Journal Of Chem. Education into different chemistry courses. These experiments introduce students to varied applications of NMR and provide them the opportunity to prepare their own samples as well as collect and process NMR data. The subject matter is first introduced in the general chemistry curriculum and students subsequently gain hands-on experience through spectroscopic identification of molecules in the organic chemistry sequence. Experiments in this sequence provide exposure to 2-D techniques and opportunities to collect and interpret data from 1-H and 13-C spectra acquired of compounds prepared in self-designed syntheses. In upper level courses and undergraduate research students perform experiments that highlight more advanced applications of FT-NMR. A longer-term goal of our project is to develop a database of student-acquired NMR data from experiments performed in the labs and to compile an accompanying laboratory manual. This should allow instructors located at institutions without access to an NMR to download raw student data from the database and process the data at their desktop. This virtual NMR allows smaller institutions the ability to provide students with real data that they have to process in a manner commonly found in large chemical research laboratories without having to buy a spectrometer.

化学（12）在三角洲州立大学，我们正在通过调整和实施在莱德大学开发的系统来创建和开发一个区域合作核磁共振设施。该设施服务于我们的机构，Coawestern社区学院，密西西比三角洲社区学院和该地区更广泛的社区。 我们的总体目标是将现代1-D和2-D FT-NMR光谱学纳入DSU，CCC和MDCC的本科化学课程。为了实现我们的目标，我们正在调整一系列的实验，主要是从化学教育杂志到不同的化学课程。这些实验向学生介绍NMR的各种应用，并为他们提供准备自己的样品以及收集和处理NMR数据的机会。该主题首先在普通化学课程中引入，学生随后通过有机化学序列中分子的光谱鉴定获得实践经验。 在这个序列中的实验提供了暴露于2-D技术和机会，收集和解释从1-H和13-C光谱获得的化合物在自行设计的合成。在高级课程和本科研究中，学生进行实验，突出FT-NMR的更先进的应用。我们的项目的一个长期目标是开发一个数据库的学生获得的NMR数据从实验室进行的实验，并编写一个附带的实验室手册。这应该允许位于无法访问NMR的机构的教师从数据库下载原始学生数据，并在桌面上处理数据。这种虚拟核磁共振使较小的机构能够为学生提供真实的数据，他们必须以大型化学研究实验室中常见的方式处理这些数据，而不必购买光谱仪。