A Regional NMR Training Cooperative with a Virtual Impact

化学(12)在三角洲州立大学，我们正在通过调整和实施莱德大学开发的系统来创建和开发一个区域合作的核磁共振设施。该设施为我们的科霍马社区学院、密西西比河三角洲社区学院和该地区更广泛的社区提供服务。我们的总体目标是将现代的一维和二维傅立叶变换核磁共振波谱技术融入到密歇根州立大学、密歇根州立大学和密歇根州立大学的本科化学课程中。为了实现我们的目标，我们主要从《化学杂志》改编了一系列实验。教育融入到不同的化学课程中。这些实验向学生介绍了核磁共振的各种应用，并为他们提供了准备自己的样品以及收集和处理核磁共振数据的机会。这一主题首先在普通化学课程中介绍，然后学生通过对有机化学序列中的分子进行光谱鉴定来获得实践经验。这一序列中的实验提供了接触2-D技术的机会，并有机会从自行设计的合成中制备的化合物的1-H和13-C光谱中收集和解释数据。在高级课程和本科生的研究中，学生进行实验，突出FT-核磁共振更高级的应用。我们项目的一个较长期的目标是开发一个学生从实验室中进行的实验中获得的核磁共振数据的数据库，并编写一份附带的实验室手册。这应该允许位于无法访问核磁共振的机构的教师从数据库下载原始学生数据，并在他们的桌面上处理数据。这种虚拟的核磁共振使较小的机构能够向学生提供真实的数据，他们必须以大型化学研究实验室常见的方式处理这些数据，而不必购买光谱仪。

Chemistry (12) At Delta State University we are creating and developing a regional cooperative NMR facility by adapting and implementing a system developed at Rider University. This facility serves our institution, Coahoma Community College, Mississippi Delta Community College and the wider community in the region. Our overarching goal is to incorporate modern 1-D and 2-D FT-NMR spectroscopy throughout the undergraduate chemistry curricula at DSU, CCC and MDCC. To achieve our goal, we are adapting a series of experiments primarily from the Journal Of Chem. Education into different chemistry courses. These experiments introduce students to varied applications of NMR and provide them the opportunity to prepare their own samples as well as collect and process NMR data. The subject matter is first introduced in the general chemistry curriculum and students subsequently gain hands-on experience through spectroscopic identification of molecules in the organic chemistry sequence. Experiments in this sequence provide exposure to 2-D techniques and opportunities to collect and interpret data from 1-H and 13-C spectra acquired of compounds prepared in self-designed syntheses. In upper level courses and undergraduate research students perform experiments that highlight more advanced applications of FT-NMR. A longer-term goal of our project is to develop a database of student-acquired NMR data from experiments performed in the labs and to compile an accompanying laboratory manual. This should allow instructors located at institutions without access to an NMR to download raw student data from the database and process the data at their desktop. This virtual NMR allows smaller institutions the ability to provide students with real data that they have to process in a manner commonly found in large chemical research laboratories without having to buy a spectrometer.