A Regional NMR Training Cooperative with a Virtual Impact

在三角洲州立大学，我们正在通过改造和实施莱德大学开发的系统，创建和开发一个区域合作核磁共振设施。该设施服务于我们的机构，科霍马社区学院，密西西比三角洲社区学院和该地区更广泛的社区。我们的总体目标是在DSU， CCC和MDCC的本科化学课程中纳入现代1-D和2-D FT-NMR光谱。为了实现我们的目标，我们正在改编一系列主要来自《化学杂志》的实验。教育分为不同的化学课程。这些实验向学生介绍核磁共振的各种应用，并为他们提供准备自己的样品以及收集和处理核磁共振数据的机会。该主题首先在普通化学课程中介绍，学生随后通过光谱识别有机化学序列中的分子获得实践经验。在这个序列的实验提供了暴露于二维技术和机会收集和解释数据从1-H和13-C光谱获得的化合物在自己设计的合成。在高级课程和本科研究学生进行实验，突出更先进的应用傅里叶核磁共振。我们项目的长期目标是开发一个从实验室进行的实验中获得的学生核磁共振数据数据库，并编写随附的实验室手册。这将允许位于没有核磁共振访问的机构的教师从数据库中下载原始学生数据，并在他们的桌面上处理数据。这种虚拟核磁共振使小型机构能够为学生提供真实的数据，他们必须以在大型化学研究实验室中常见的方式处理这些数据，而不必购买光谱仪。

Chemistry (12) At Delta State University we are creating and developing a regional cooperative NMR facility by adapting and implementing a system developed at Rider University. This facility serves our institution, Coahoma Community College, Mississippi Delta Community College and the wider community in the region. Our overarching goal is to incorporate modern 1-D and 2-D FT-NMR spectroscopy throughout the undergraduate chemistry curricula at DSU, CCC and MDCC. To achieve our goal, we are adapting a series of experiments primarily from the Journal Of Chem. Education into different chemistry courses. These experiments introduce students to varied applications of NMR and provide them the opportunity to prepare their own samples as well as collect and process NMR data. The subject matter is first introduced in the general chemistry curriculum and students subsequently gain hands-on experience through spectroscopic identification of molecules in the organic chemistry sequence. Experiments in this sequence provide exposure to 2-D techniques and opportunities to collect and interpret data from 1-H and 13-C spectra acquired of compounds prepared in self-designed syntheses. In upper level courses and undergraduate research students perform experiments that highlight more advanced applications of FT-NMR. A longer-term goal of our project is to develop a database of student-acquired NMR data from experiments performed in the labs and to compile an accompanying laboratory manual. This should allow instructors located at institutions without access to an NMR to download raw student data from the database and process the data at their desktop. This virtual NMR allows smaller institutions the ability to provide students with real data that they have to process in a manner commonly found in large chemical research laboratories without having to buy a spectrometer.