Improvement of Resolution of a Electron Microscope by Means of Correction of Spherical Aberration Using a Foil Lens
Improvement of Resolution of a Electron Microscope by Means of Correction of Spherical Aberration Using a Foil Lens
批准号:
11650055
负责人:
HANAI Takaaki
金额:
$2.24万
依托单位:
依托单位国家:
日本
项目类别:
Grant-in-Aid for Scientific Research (C)
财政年份:
1999
资助国家:
日本
项目状态:
已结题
起止时间:
1999 至 2000
中文摘要
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英文摘要
1. Development of a foil lens for the objective lens of a transmission electron microscope (TEM).In order to design the foil lens which enables us to correct the spherical aberration at a lower electrostatic field than 120 kV/mm, that is the known limit of self-supporting of the foil electrode, optical characteristics of the foil lens were numerically studied. It was found that that the correction is achieved by locating the foil lens at the position 3.6 mm lower from the center of the gap of the objective polepieces. The spherical aberration is corrected at the foil lens voltage of 550 V when the distance of the aperture and foil electrodes. An improved side-entry type foil lens was developed based on the calculation. The foil lens holder has the thickness of 1.7 mm, 0.3 mm thinner than previous one.2. Observation of crystal lattice images with the improved foil lens.The foil lens was incorporated with a commercial TEM and the images of Au fine particles were observed at the accelerating voltage of 200 kV. At the foil lens voltage of 300 V, (111) lattice images were observed at nearly in-focus condition where the contrast of the Fresnel fringe was weak. Such reduction of aretefacts shows an effect of correction of spherical aberration.3. Measurements of spherical aberration of the corrected objective lens.The spherical aberration was measured with a newly developed method, in which the spherical aberration coefficient and the defocus are simultaneously determined from the deviation of the dark-field TEM images of Au particles from the corresponding bright-field image. It was shown that the improved foil lend yields smaller spherical aberration coefficients than the previous one at the same foil lens voltage.
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Electron beam-induced chemical reactions of single crystal calcium floride by time-resolved EELS
时间分辨 EELS 电子束诱导单晶氟化钙化学反应
DOI:
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发表时间:
2000
期刊:
Microscopy and Microanalysis 6(suppl. 2)
影响因子:
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作者:
[室岡義栄]
通讯作者:
室岡義栄
"As-quenched Arc Products by Pules-Discharg"Microscopy & Microanalysis 2000. 6・suppl.2. 54-55 (2000)
“脉冲放电的淬火电弧产品”Microscopy & Microanalysis 2000. 6・suppl.2 (2000)
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室岡義栄: "As-quenched arc products by pulse-discharge"Microscopy & Microanalysis 2000. (発表予定). (2000)
Yoshihide Murooka:“脉冲放电淬火电弧产品”Microscopy & Microanalysis 2000。(待提交)。
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Pulse-arc system for investigation of initial fullerene deposition.
用于研究初始富勒烯沉积的脉冲电弧系统。
DOI:
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发表时间:
2000
期刊:
Microscopy and Microanalysis 6(suppl. 2)
影响因子:
--
作者:
[室岡義栄]
通讯作者:
室岡義栄
花井孝明: "Maximum Entropy Restoration of Electron Microscope Images with a Random-Spatial-Distribution Constraint (印刷中)"Scanning Electron Microscopy. 11・suppl.. 377-388 (2000)
Takaaki Hanai:“具有随机空间分布约束的电子显微镜图像的最大熵恢复(正在出版)”扫描电子显微镜11·suppl.. 377-388(2000)
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共 19 条
Research on a Structure Analysis of Materials with a Maximum Entropy Restoration of Electron Microscope Images.
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批准号:09650063
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项目类别:Grant-in-Aid for Scientific Research (C)
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资助金额:$2.05万
-
财政年份:1997
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负责人:HANAI Takaaki
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依托单位:
Research on an Improvement of Resolution of Electron Microscope by Means of Maximum Entropy Image Restoration.
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批准号:07650395
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项目类别:Grant-in-Aid for Scientific Research (C)
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资助金额:$1.34万
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财政年份:1995
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负责人:HANAI Takaaki
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依托单位:
Development of a high resolution scanning transmission electron microscope with a foil lens for correction of spherical aberration
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批准号:05555099
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项目类别:Grant-in-Aid for Developmental Scientific Research (B)
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资助金额:$4.74万
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财政年份:1993
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负责人:HANAI Takaaki
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依托单位:
Fundamental study on spherical aberration correction of the objective lens of an electron microscope using a foil lens
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批准号:05650051
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项目类别:Grant-in-Aid for General Scientific Research (C)
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资助金额:$1.54万
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财政年份:1993
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负责人:HANAI Takaaki
-
依托单位:
海外基金