COURSES IN SEPARATION & CHARACTERIZATION OF COMPLEX CARBOHYDRATES
分离课程
基本信息
- 批准号:6653606
- 负责人:
- 金额:$ 28.8万
- 依托单位:
- 依托单位国家:美国
- 项目类别:
- 财政年份:2002
- 资助国家:美国
- 起止时间:2002-08-01 至 2003-07-31
- 项目状态:已结题
- 来源:
- 关键词:
项目摘要
Glycosyl composition analysis was performed on Ehrlichia risticii
lipopolysaccharides. The samples were analyzed for monosaccharide
composition by preparing the trimethylsilyl derivatives of the
methylglycosides followed by gas chromatography (GC) and combined gas
chromatography/mass spectrometry (GC-MS) analysis. TMS
methylglycosides were prepared from the sample by methanolysis in 3 M
HCl followed by N-acetylation with pyridine and acetic anhydride. The
samples were then treated with Tri-Sil. GC analysis of the TMS
methylglycosides was done on an HP5890 GC using a DB1 fused silica
capillary column. GC-MS analysis was performed using an HP5890 GC
coupled to a 5970 MSD. Monosaccharides were identified by their
retention times in comparison to standards, and the carbohydrate
character of these was authenticated by their mass spectra.
对氏埃利希菌进行了糖基组成分析
项目成果
期刊论文数量(0)
专著数量(0)
科研奖励数量(0)
会议论文数量(0)
专利数量(0)
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ROBERTA K MERKLE其他文献
ROBERTA K MERKLE的其他文献
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{{ truncateString('ROBERTA K MERKLE', 18)}}的其他基金
GLYCOSYL COMPOSITION ANALYSIS OF MANDUCA SEXTA CHITINASE
烟草天蛾几丁质酶的糖基组成分析
- 批准号:
6653603 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
GLYCOSYL COMPOSITION ANALYSIS OF GLYCOPROTEIN SAMPLES
糖蛋白样品的糖基组成分析
- 批准号:
6653593 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
GLYCOSYL LINKAGE ANALYSIS OF ENZYMATICALLY SYNTHESIZED GLUCANS
酶法合成葡聚糖的糖基连接分析
- 批准号:
6653598 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
GLYCOSYL COMPOSITION ANALYSIS OF COLLAGEN SAMPLES
胶原蛋白样品的糖基成分分析
- 批准号:
6653591 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
GLYCOSYL COMPOSITION ANALYSIS OF STREPTOCOCCUS SUIS
猪链球菌的糖基组成分析
- 批准号:
6653590 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
GLYCOSYL LINKAGE ANALYSIS OF WATER SOLUBLE & INSOLUBLE LINKED GLUCANS
水溶性的糖基连接分析
- 批准号:
6653599 - 财政年份:2002
- 资助金额:
$ 28.8万 - 项目类别:
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